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Chemistry
Heterocyclic Building Blocks
Benzothiophenes
Benzo[b]thiophen-5-ylmethanol
Chemistry
Heterocyclic Building Blocks
Organic Building Blocks
Benzothiophenes
Alcohols

[ CAS No. 20532-34-7 ] {[proInfo.proName]}

,{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]}
Chemical Structure| 20532-34-7
Chemical Structure| 20532-34-7
Structure of 20532-34-7 * Storage: {[proInfo.prStorage]}

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Quality Control of [ 20532-34-7 ]

COA NMR CNMR HPLC LC-MS

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SDS Specification
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Product Citations

Product Details of [ 20532-34-7 ]

CAS No. :20532-34-7 MDL No. :MFCD04972640
Formula : C9H8OS Boiling Point : No data available
Linear Structure Formula :- InChI Key :JSYSQUAJOCDMJW-UHFFFAOYSA-N
M.W : 164.22 Pubchem ID :2795446
Synonyms :

Safety of [ 20532-34-7 ]

Signal Word:Warning Class:
Precautionary Statements:P261-P305+P351+P338 UN#:
Hazard Statements:H315-H319-H335 Packing Group:
GHS Pictogram:

Application In Synthesis of [ 20532-34-7 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 20532-34-7 ]

[ 20532-34-7 ] Synthesis Path-Downstream   1~8

  • 1
  • [ 20532-34-7 ]
  • [ 74-88-4 ]
  • [ 96803-56-4 ]
YieldReaction ConditionsOperation in experiment
70% With potassium hydroxide; In dimethyl sulfoxide; Step A Preparation of 5-Methoxymethylbenzo [b]thiophene To a stirred mixture of powdered KOH (18.9 g, 0.336 mol) in dimethylsulfoxide (100 ml) was added <strong>[20532-34-7]5-hydroxymethylbenzo[b]thiophene</strong> (13.8 g, 0.084 mol) in 25 ml of dimethylsulfoxide. Then methyl iodide (23.9 g, 0.168 mol) was added dropwise at ambient temperature over several minutes. Stirring was continued for 11/2 hours. The mixture was filtered, diluted with water (150 ml) and extracted with methylene chloride (200 ml) in three portions. The combined extracts were washed with water, dried over anhydrous Na2 SO4, filtered and concentrated in vacuo. This gave 14.1 g of amber liquid. Distillation gave 10.47 g of colorless liquid, b.p. 2.2 mm Hg 110-111 C. (Yield 70%).
Reference： [1]Journal of Medicinal Chemistry,1989,vol. 32,p. 2548 - 2554
[2]Patent: US4668697,1987,A
  • 2
  • [ 10133-22-9 ]
  • [ 20532-34-7 ]
  • [ 10133-30-9 ]
  • sodium; benzo[<i>b</i>]thiophen-5-yl-methanesulfonate [ No CAS ]
Reference： [1]Synthetic Communications,2003,vol. 33,p. 627 - 632
  • 3
  • [ 20532-34-7 ]
  • [ 96803-63-3 ]
Reference： [1]Journal of Medicinal Chemistry,1989,vol. 32,p. 2548 - 2554
  • 4
  • [ 20532-34-7 ]
  • [ 96803-58-6 ]
Reference： [1]Journal of Medicinal Chemistry,1989,vol. 32,p. 2548 - 2554
  • 5
  • [ 20532-34-7 ]
  • [ 96803-57-5 ]
Reference： [1]Journal of Medicinal Chemistry,1989,vol. 32,p. 2548 - 2554
  • 6
  • [ 20532-34-7 ]
  • [ 96803-59-7 ]
Reference： [1]Journal of Medicinal Chemistry,1989,vol. 32,p. 2548 - 2554
  • 7
  • [ 20532-34-7 ]
  • [ 96803-62-2 ]
Reference： [1]Journal of Medicinal Chemistry,1989,vol. 32,p. 2548 - 2554
  • 8
  • [ 20532-34-7 ]
  • [ 96803-11-1 ]
Reference： [1]Journal of Medicinal Chemistry,1989,vol. 32,p. 2548 - 2554

Tags: 20532-34-7 synthesis path| 20532-34-7 SDS| 20532-34-7 COA| 20532-34-7 purity| 20532-34-7 application| 20532-34-7 NMR| 20532-34-7 COA| 20532-34-7 structure

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Organic Building Blocks
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Technical Information

• Appel Reaction • Buchwald-Hartwig C-N Bond and C-O Bond Formation Reactions • Chugaev Reaction • Corey-Kim Oxidation • Dess-Martin Oxidation • Hydride Reductions • Jones Oxidation • Martin's Sulfurane Dehydrating Reagent • Mitsunobu Reaction • Moffatt Oxidation • Oxidation of Alcohols by DMSO • Preparation of Alcohols • Preparation of Amines • Reactions of Alcohols • Reactions with Organometallic Reagents • Ritter Reaction • Sharpless Olefin Synthesis • Swern Oxidation
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