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Chemical Structure| 208261-83-0 Chemical Structure| 208261-83-0

Structure of 208261-83-0

Chemical Structure| 208261-83-0

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Product Details of [ 208261-83-0 ]

CAS No. :208261-83-0
Formula : C9H7BrN2O
M.W : 239.07
SMILES Code : COC1=C2N=CC=NC2=C(Br)C=C1
MDL No. :MFCD28661900

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Application In Synthesis of [ 208261-83-0 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 208261-83-0 ]

[ 208261-83-0 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 124-41-4 ]
  • [ 148231-12-3 ]
  • [ 208261-83-0 ]
YieldReaction ConditionsOperation in experiment
310 mg With copper(l) iodide; In methanol; N,N-dimethyl-formamide; at 100℃; for 18h; A solution of <strong>[148231-12-3]5,8-dibromoquinoxaline</strong> (800 mg, 2.78 mmol), cuprous iodide (529 mg, 2.78 mmol), sodium methoxide (5.4 M in MeOH, 0.57 mL, 3.06 mmol) in DMF (20 mL) was stirred at 100 C for 18 hrs. After concentration, the mixture was purified by flash column (PE/EA = 2/1) to give compound HI (310 mg) as a yellow solid. MS calc?d 239 (MH+), measured 239 (MH+).
 

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