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CAS No. : | 2159132-86-0 | MDL No. : | N/A |
Formula : | C44H28N4 | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | YVQFZWONVSMZFO-UHFFFAOYSA-N |
M.W : | 612.72 | Pubchem ID : | 132164939 |
Synonyms : |
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Signal Word: | Warning | Class: | |
Precautionary Statements: | P261-P280-P301+P312-P302+P352-P305+P351+P338 | UN#: | |
Hazard Statements: | H302-H315-H319-H335 | Packing Group: | |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
77% | Stage #1: 5,8-dihydro-5-phenyl-5,8-diazaindeno[2,1-c]fluorene With sodium hydride In N,N-dimethyl-formamide for 1h; Stage #2: 4-([1,1′-biphenyl]-4-yl)-2-chloroquinazoline In N,N-dimethyl-formamide at 20℃; | Compound Cmp D-2 was synthesized A 3-necked round flask was charged with 5-phenyl-5,8-dihydroindolo [2,3-c] carbazole (5 g, 15.04 mmol).Anhydrous DMF (100 ml) was added to it.To this clear solution was added sodium hydride (1.203 g, 30.1 mmol).The resulting mixture was stirred for 1 hour.Then 4 - ([1,1'-biphenyl] -4-yl) -2-chloroquinazoline (5.72 g, 18.05 mmol)And the resulting mixture was stirred at room temperature overnight.The reaction mixture was quenched with ice / cold H 2 O (1.5 L).The resulting mixture was stirred for 30 minutes.The yellow solid was filtered and washed with H20 (1 L).The solid was dried, suspended in toluene (500 mL), heated, and stirred for 30 minutes. The suspension is warmed again and filtered.The solid was washed with toluene and passed through a plug of silica.This compound was suspended in DCM (100 mL) and acetone (250 mL).The suspension is heated and then stirred at room temperature overnight.It was filtered and washed with acetone (200 mL).The solid was dried under vacuum,5- (4 - ([1,1'-biphenyl] -4-yl) quinazolin- 2-yl) -8- phenyl- 5,8-dihydroindolo [2,3-c ] Carbazole (7.1 g, 77% yield, HPLC 99.99%). |
[ 1831056-76-8 ]
7-(4-(9-Phenyl-9H-carbazol-2-yl)quinazolin-2-yl)-7H-dibenzo[c,g]carbazole
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