Home Cart 0 Sign in  

[ CAS No. 22224-41-5 ] {[proInfo.proName]}

,{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]}
Chemical Structure| 22224-41-5
Chemical Structure| 22224-41-5
Structure of 22224-41-5 * Storage: {[proInfo.prStorage]}
Cart0 Add to My Favorites Add to My Favorites Bulk Inquiry Inquiry Add To Cart

Quality Control of [ 22224-41-5 ]

Related Doc. of [ 22224-41-5 ]

Alternatived Products of [ 22224-41-5 ]

Product Details of [ 22224-41-5 ]

CAS No. :22224-41-5 MDL No. :MFCD00080818
Formula : C26H22O8 Boiling Point : -
Linear Structure Formula :- InChI Key :HUHVPBKTTFVAQF-PIXQIBFHSA-N
M.W : 462.45 Pubchem ID :11005061
Synonyms :
1,3,5-Tri-O-benzoyl-a-D-ribofuranose
Chemical Name :1,3,5-Tri-O-benzoyl-a-D-ribofuranose

Safety of [ 22224-41-5 ]

Signal Word:Warning Class:N/A
Precautionary Statements:P280-P305+P351+P338 UN#:N/A
Hazard Statements:H302 Packing Group:N/A
GHS Pictogram:

Application In Synthesis of [ 22224-41-5 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Upstream synthesis route of [ 22224-41-5 ]
  • Downstream synthetic route of [ 22224-41-5 ]

[ 22224-41-5 ] Synthesis Path-Upstream   1~17

  • 1
  • [ 6974-32-9 ]
  • [ 22224-41-5 ]
YieldReaction ConditionsOperation in experiment
65.1% With hydrogenchloride In dichloromethane for 2.5 h; Cooling with ice The synthesis of compound vi: The compound v (2.57mmol) was dissolved in 26 ml dry dichloromethane and dry HCl gas was slowly introduced into an ice-water bath for 2.5 hours. The solution was washed with 19.5ml ice water and the organic layer was separated. The organic layer was washed with saturated sodium bicarbonate until the water layer shows weak alkaline, and then washed with ice water until the water layer shows neutral, dried over anhydrous sodium sulfate for more than 4 hours, and then drawn off under a reduced pressure to obtain light yellow syrup. The syrup was recrystallized using the mixed solvent of hexane and dichloromethane, so as to obtain the white solid compound vi (65.1percent). 1H NMR(CDCl3) δppm: 7.36.similar.8.14 (m, 15H, OBz), 6.68 (d, J=4.4Hz, 1H, H-1), 5.59 (dd, 1H, H-3), 4.64.similar.4.80 (m, 4H, H-2, H-4 and H-5). M,p, 139.similar.140°C.
Reference: [1] Patent: EP2177527, 2010, A1, . Location in patent: Page/Page column 11
[2] Journal of Organic Chemistry, 1985, vol. 50, # 14, p. 2597 - 2598
  • 2
  • [ 6974-32-9 ]
  • [ 115459-50-2 ]
  • [ 22224-41-5 ]
Reference: [1] Journal of Organic Chemistry, 1988, vol. 53, p. 85 - 88
  • 3
  • [ 16205-60-0 ]
  • [ 115459-50-2 ]
  • [ 22224-41-5 ]
Reference: [1] Journal of Organic Chemistry, 1985, vol. 50, # 14, p. 2597 - 2598
  • 4
  • [ 55797-81-4 ]
  • [ 108-24-7 ]
  • [ 22224-41-5 ]
Reference: [1] Journal of the American Chemical Society, 1954, vol. 76, p. 1663,1666
  • 5
  • [ 69350-76-1 ]
  • [ 22224-41-5 ]
Reference: [1] Journal of Organic Chemistry, 1985, vol. 50, # 14, p. 2597 - 2598
  • 6
  • [ 79439-67-1 ]
  • [ 22224-41-5 ]
Reference: [1] Carbohydrate Research, 2000, vol. 324, # 3, p. 149 - 160
  • 7
  • [ 98-88-4 ]
  • [ 58-61-7 ]
  • [ 22224-41-5 ]
Reference: [1] Chemische Berichte, 1952, vol. 85, p. 1000,1005
  • 8
  • [ 532-31-0 ]
  • [ 73611-06-0 ]
  • [ 71-43-2 ]
  • [ 98796-65-7 ]
  • [ 22224-41-5 ]
Reference: [1] Journal of Organic Chemistry, 1957, vol. 22, p. 1465,1468
[2] Journal of the American Chemical Society, 1956, vol. 78, p. 4710,4714 Anm. 19[3] Journal of Organic Chemistry, 1957, vol. 22, p. 1465,1468
  • 9
  • [ 189129-08-6 ]
  • [ 16352-06-0 ]
  • [ 62374-52-1 ]
  • [ 67525-66-0 ]
  • [ 189129-04-2 ]
  • [ 105330-91-4 ]
  • [ 22224-41-5 ]
Reference: [1] Nucleosides and Nucleotides, 1997, vol. 16, # 1-2, p. 129 - 144
  • 10
  • [ 105330-91-4 ]
  • [ 16352-06-0 ]
  • [ 62374-52-1 ]
  • [ 67525-66-0 ]
  • [ 189129-04-2 ]
  • [ 22224-41-5 ]
Reference: [1] Nucleosides and Nucleotides, 1997, vol. 16, # 1-2, p. 129 - 144
  • 11
  • [ 189129-04-2 ]
  • [ 16352-06-0 ]
  • [ 62374-52-1 ]
  • [ 67525-66-0 ]
  • [ 105330-91-4 ]
  • [ 22224-41-5 ]
Reference: [1] Nucleosides and Nucleotides, 1997, vol. 16, # 1-2, p. 129 - 144
  • 12
  • [ 189129-08-6 ]
  • [ 16352-06-0 ]
  • [ 62374-52-1 ]
  • [ 67525-66-0 ]
  • [ 189129-04-2 ]
  • [ 105330-91-4 ]
  • [ 22224-41-5 ]
Reference: [1] Nucleosides and Nucleotides, 1997, vol. 16, # 1-2, p. 129 - 144
  • 13
  • [ 105330-91-4 ]
  • [ 16352-06-0 ]
  • [ 62374-52-1 ]
  • [ 67525-66-0 ]
  • [ 189129-04-2 ]
  • [ 22224-41-5 ]
Reference: [1] Nucleosides and Nucleotides, 1997, vol. 16, # 1-2, p. 129 - 144
  • 14
  • [ 189129-04-2 ]
  • [ 16352-06-0 ]
  • [ 62374-52-1 ]
  • [ 67525-66-0 ]
  • [ 105330-91-4 ]
  • [ 22224-41-5 ]
Reference: [1] Nucleosides and Nucleotides, 1997, vol. 16, # 1-2, p. 129 - 144
  • 15
  • [ 22224-41-5 ]
  • [ 2140-72-9 ]
Reference: [1] Journal of Organic Chemistry, 1982, vol. 47, # 2, p. 202 - 206
  • 16
  • [ 22224-41-5 ]
  • [ 69256-17-3 ]
Reference: [1] Nucleosides, nucleotides and nucleic acids, 2003, vol. 22, # 5-8, p. 1343 - 1346
  • 17
  • [ 22224-41-5 ]
  • [ 97614-43-2 ]
Reference: [1] Nucleosides, nucleotides and nucleic acids, 2003, vol. 22, # 5-8, p. 1343 - 1346
[2] Journal of the American Chemical Society, 1995, vol. 117, # 43, p. 10781 - 10782
[3] Organic Letters, 2004, vol. 6, # 9, p. 1465 - 1468
[4] Tetrahedron, 1998, vol. 54, # 28, p. 8223 - 8240
[5] Tetrahedron, 2012, vol. 68, # 26, p. 5145 - 5151
Recommend Products
Same Skeleton Products
Historical Records