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Chemical Structure| 23474-98-8 Chemical Structure| 23474-98-8

Structure of 23474-98-8

Chemical Structure| 23474-98-8

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Product Details of [ 23474-98-8 ]

CAS No. :23474-98-8
Formula : C6H6ClNS
M.W : 159.64
SMILES Code : SC1=CC(Cl)=CC=C1N
MDL No. :MFCD03094703
InChI Key :TYRZAGMAVZESQX-UHFFFAOYSA-N
Pubchem ID :2737518

Safety of [ 23474-98-8 ]

GHS Pictogram:
Signal Word:Danger
Hazard Statements:H315-H318-H335
Precautionary Statements:P261-P264-P271-P280-P302+P352-P304+P340-P305+P351+P338-P310-P332+P313-P362-P403+P233-P405-P501
Class:8
UN#:1759
Packing Group:

Application In Synthesis of [ 23474-98-8 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 23474-98-8 ]

[ 23474-98-8 ] Synthesis Path-Downstream   1~5

  • 1
  • [ 23474-98-8 ]
  • [ 50995-48-7 ]
  • [ 139331-33-2 ]
  • 2
  • [ 23474-98-8 ]
  • [ 4494-26-2 ]
  • C16H16ClN3O5S [ No CAS ]
  • 3
  • [ 23474-98-8 ]
  • [ 15119-34-3 ]
  • [ 1360807-33-5 ]
  • 4
  • [ 23474-98-8 ]
  • [ 608-21-9 ]
  • C12H7BrClNS [ No CAS ]
YieldReaction ConditionsOperation in experiment
41% With polyphosphoric acid; at 180℃; for 4h; 2-amino-5-chlorobenzenethiol (2.4 g, 0.010 mol) in <strong>[608-21-9]1,2,3-tribromobenzene</strong>6 (3.7 g, 0.012 mol) by the insert synthesized in the same manner used in Example 25-Preparation Example 1 to give the 1.3 g (yield 41%). (m / z = 312) 2-amino-5-chlorophenol (3.0 g, 0.014 mol) in <strong>[608-21-9]1,2,3-tribromobenzene</strong> (4.4 g, 0.014 mol) into a PPA (polyphosphoric acid) into 100 mL to 180 C 4 hours reaction was stirred. After the reaction cooled H20: MC column purification (n-Hexane: MC) to give the intermediate 25-1 2.1 g (51%) (m / z = 296).
  • 5
  • [ 23474-98-8 ]
  • [ 608-21-9 ]
  • C13H6BrClN2S [ No CAS ]
 

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