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CAS No. : | 24211-54-9 | MDL No. : | MFCD06202374 |
Formula : | C5H9NO2 | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | GPRZVNYVEZZOKH-BYPYZUCNSA-N |
M.W : | 115.13 | Pubchem ID : | 10964456 |
Synonyms : |
|
Signal Word: | Warning | Class: | N/A |
Precautionary Statements: | P261-P264-P270-P271-P280-P301+P312-P302+P352-P304+P340-P305+P351+P338-P330-P332+P313-P337+P313-P362-P403+P233-P405-P501 | UN#: | N/A |
Hazard Statements: | H302-H315-H319-H335 | Packing Group: | N/A |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
98% | With 20% palladium hydroxide-activated charcoal; hydrogen In methanol at 25℃; for 24 h; | To a solution of azide 13 (1.5 g, 10.62 mmol) in dry MeOH was added 20percent Pd(OH)2 (0.037 g, 0.53 mmol) and the reaction mixture was stirred under an atmosphere of H2 (1 atm) for 24 h at 25 oC. After completion of the reaction (monitored by TLC), the catalyst was filtered over Celite and the filtrate concentrated under reduced pressure to provide crude hydroxylactam, which was purified by column chromatography using ethyl acetate:methanol (9:1) as eluent to obtain pure hydroxylactam 14 (1.19 g, 98percent). |
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