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Chemistry
Organic Building Blocks
Aryls
N1-(4-Methoxyphenyl)ethane-1,2-diamine
Chemistry
Organic Building Blocks
Aryls
Amines Ethers Benzene Compounds

[ CAS No. 24455-93-4 ] {[proInfo.proName]}

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Cat. No.: {[proInfo.prAm]}
Chemical Structure| 24455-93-4
Chemical Structure| 24455-93-4
Structure of 24455-93-4 * Storage: {[proInfo.prStorage]}
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Quality Control of [ 24455-93-4 ]

COA NMR CNMR HPLC LC-MS

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SDS Specification
Alternatived Products of [ 24455-93-4 ]

Product Details of [ 24455-93-4 ]

CAS No. :24455-93-4 MDL No. :MFCD06795942
Formula : C9H14N2O Boiling Point : -
Linear Structure Formula :- InChI Key :-
M.W : 166.22 Pubchem ID :-
Synonyms :

Safety of [ 24455-93-4 ]

Signal Word: Class:
Precautionary Statements: UN#:
Hazard Statements: Packing Group:

Application In Synthesis of [ 24455-93-4 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 24455-93-4 ]

[ 24455-93-4 ] Synthesis Path-Downstream   1~8

  • 1
  • [ 497-25-6 ]
  • [ 20265-97-8 ]
  • [ 24455-93-4 ]
YieldReaction ConditionsOperation in experiment
In ethoxyethoxyethanol; at 150℃; for 0.166667h;Microwave irradiation; A solution of 2-oxazolidinone (1.5 g, 17.2 mmol) in 2-(2-ethoxyethoxy)ethanol (20 mL) was treated with <strong>[20265-97-8]p-anisidine hydrochloride</strong> (2.1 g, 17.2 mmol) and heated in the microwave at 150 C. at 300 W for 10 min. The solution was cooled to rt and Et2O (50 mL) was added. The resulting solid precipitate was filtered and washed with Et2O (3×20 mL). HPLC: Rt=0.23. MS (ESI): mass calcd. for C9H14N2O, 166.1; m/z found, 150 [M-16]+.
Reference： [1]Journal of Organic Chemistry,1992,vol. 57,p. 6257 - 6265
[2]Patent: US2008/207683,2008,A1 .Location in patent: Page/Page column 12
  • 2
  • [ 24455-93-4 ]
  • [ 102410-65-1 ]
  • [ 99-04-7 ]
  • (S)-N-[2-(4-methoxyphenylamino)ethylcarbamoyl]phenylmethyl}-3-methylbenzamide [ No CAS ]
Reference： [1]Bioorganic and Medicinal Chemistry Letters,2005,vol. 15,p. 4979 - 4984
  • 3
  • [ 24455-93-4 ]
  • [ 77128-72-4 ]
  • [ 99-04-7 ]
  • (S)-N-{2-(4-methoxyphenyl)-1-[2-(4-methoxyphenylamino)ethylcarbamoyl]ethyl}-3-methylbenzamide [ No CAS ]
Reference： [1]Bioorganic and Medicinal Chemistry Letters,2005,vol. 15,p. 4979 - 4984
  • 4
  • [ 24455-93-4 ]
  • [ 169555-95-7 ]
  • [ 99-04-7 ]
  • (S)-N-{1-[2-(4-methoxyphenylamino)ethylcarbamoyl]-2-pyridin-4-ylethyl}-3-methylbenzamide [ No CAS ]
Reference： [1]Bioorganic and Medicinal Chemistry Letters,2005,vol. 15,p. 4979 - 4984
  • 5
  • [ 24455-93-4 ]
  • [ 199110-64-0 ]
  • [ 99-04-7 ]
  • (S)-N-{2-biphenyl-4-yl-1-[2-(4-methoxyphenylamino)ethylcarbamoyl]ethyl}-3-methylbenzamide [ No CAS ]
Reference： [1]Bioorganic and Medicinal Chemistry Letters,2005,vol. 15,p. 4979 - 4984
  • 6
  • [ 24455-93-4 ]
  • [ 99-04-7 ]
  • [ 159611-02-6 ]
  • <i>N</i>-{2-furan-2-yl-1-[2-(4-methoxy-phenylamino)-ethylcarbamoyl]-ethyl}-3-methyl-benzamide [ No CAS ]
Reference： [1]Bioorganic and Medicinal Chemistry Letters,2005,vol. 15,p. 4979 - 4984
  • 7
  • [ 24455-93-4 ]
  • [ 530-62-1 ]
  • [ 62868-39-7 ]
YieldReaction ConditionsOperation in experiment
44% In tetrahydrofuran Heating;
Reference： [1]Llopart, Carme Cantos; Ferrer, Conchita; Joule, John A. [Canadian Journal of Chemistry, 2004, vol. 82, # 11, p. 1649 - 1661]
  • 8
  • [ 497-25-6 ]
  • [ 111-77-3 ]
  • [ 20265-97-8 ]
  • [ 24455-93-4 ]
YieldReaction ConditionsOperation in experiment
45% EXAMPLE 9 Preparation of N-(4-Methoxyphenyl)-1,2-ethanediamine A mixture of 4-methoxyaniline hydrochloride (17.1 g, 0.107 mole), 2-oxazolidinone (8.7 g, 0.10 mole) and 50 ml of 2-(2-methoxyethoxy)ethanol was heated to 175 C. After five hours, carbon dioxide gas evolution had ceased and the dark mixture was allowed to cool to room temperature. Neutralization in a manner similar to that described in Example 1, and distillation at 130 C. to 140 C. (0.5 mm Hg) afforded a 45 percent yield of the amine as a colorless liquid which slowly solidified on standing at ambient temperature to a low-melting solid.
Reference： [1]Patent: US4381401,1983,A

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