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Chemical Structure| 24782-25-0 Chemical Structure| 24782-25-0

Structure of 24782-25-0

Chemical Structure| 24782-25-0

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Product Details of [ 24782-25-0 ]

CAS No. :24782-25-0
Formula : C13H13NO3
M.W : 231.25
SMILES Code : O=C(C1=NC2=CC=CC=C2C(OC)=C1)OCC

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Application In Synthesis of [ 24782-25-0 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 24782-25-0 ]

[ 24782-25-0 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 368-39-8 ]
  • [ 5965-59-3 ]
  • [ 24782-25-0 ]
YieldReaction ConditionsOperation in experiment
81% With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20℃; for 48.0h; General procedure: A mixture of 4-oxo-1,4-dihydroquinoline-2-carboxylic acid alkylester (1, 1 mmol), base (1.3 mmol), the corresponding alkylatingagent (alkyl iodide, 1.5 mmol; others, 1.2 mmol) and anhydrousDMF (5 mL) was stirred at the appropriate temperature andmonitored by TLC (DCM:MeOH 4.7:0.3). After a specified time(Table 2), the mixture was carefully poured into ice-water. Thecompounds obtained were isolated and purified as was indicatedabove. Alkylating agents, bases and solvents are presented inTable 2.
 

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