2598-31-4|1-(8-Hydroxyquinolin-5-yl)ethanone| Ambeed

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Quality Control of [ 2598-31-4 ] Purity: 98% SDS Specification

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Product Details of [ 2598-31-4 ]

CAS No. :	2598-31-4
Formula :	C₁₁H₉NO₂
M.W :	187.19
SMILES Code :	CC(C1=C2C=CC=NC2=C(O)C=C1)=O
MDL No. :	MFCD00086061
InChI Key :	HZTCLDNADGMACV-UHFFFAOYSA-N
Pubchem ID :	95877

Safety of [ 2598-31-4 ]

GHS Pictogram:
Signal Word:	Warning
Hazard Statements:	H302-H315-H319
Precautionary Statements:	P261-P305+P351+P338

Application In Synthesis of [ 2598-31-4 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

Downstream synthetic route of [ 2598-31-4 ]

[ 2598-31-4 ] Synthesis Path-Downstream 1~37

1
[ 110-89-4 ]
[ 50-00-0 ]
[ 2598-31-4 ]
[ 107456-81-5 ]

References: [1]Journal of the American Chemical Society,1952,vol. 74,p. 5209.

2
[ 98-01-1 ]
[ 2598-31-4 ]
[ 101727-41-7 ]

References: [1]Journal of the Indian Chemical Society,1990,vol. 67,p. 821 - 823.
[2]Patent: US2770619,1954,A .

3
[ 148-24-3 ]
[ 75-36-5 ]
[ 2598-31-4 ]

Yield	Reaction Conditions	Operation in experiment
55%	With aluminum (III) chloride; titanium tetrachloride; In nitrobenzene; at 70℃; for 12h;	To a solution of acetyl chloride (2) (1.62 g, 20 mmol) in nitrobenzene (3-5mL), introduce 8-hydroxyquinoline (1) (3 g, 20 mmol), a yellow folculant precipitate out. To a above reaction mixture, added about 5 g aluminium chloride/titanium chloride with constant shaking, the precipitate disappeared and a clear semi-solid was resulted. It was kept at 70 C for 12 h in a flask fitted with a calcium chloride tube. On cooling, some crushed ice and 100 mL 10% HCl was added to it and the separated nitrobenzene was driven off with steam. On standing overnight, the separated hydrochloride of 5-acetyl-8-hydroxyquinoline (3) was filtered. It was dissolved in water and on the addition of sodium acetate to it, the free base separated out. It was recrystallized from hot water; (55% of the theoretical) after recrystallization. Compound 3 is colourless hair-like needles from hot water (Scheme-I). Yield 55%; m.p.: 112-114 C; MS m/z: 187.06 (100.0%) (M+); Anal. calcd. (found) for C11H9NO2 (%): C, 70.58 (70.51); H,4.85 (4.78); N, 7.48 (7.43).

References: [1]Bulletin of the Chemical Society of Japan,1987,vol. 60,p. 2327 - 2334.
[2]Asian Journal of Chemistry,2020,vol. 32,p. 1609 - 1613.
[3]Beilstein Journal of Organic Chemistry,2014,vol. 10,p. 2038 - 2054.
[4]Archiv der Pharmazie,1941,vol. 279,p. 154,164.
[5]Pharmazie,1985,vol. 40,p. 307 - 311.

4
[ 120-57-0 ]
[ 2598-31-4 ]
[ 109941-53-9 ]

References: [1]Journal of the American Chemical Society,1931,vol. 53,p. 1493,1495.

5
[ 50-00-0 ]
[ 2598-31-4 ]
[ 102546-93-0 ]

References: [1]Journal of the American Chemical Society,1931,vol. 53,p. 1493,1495.

6
[ 2598-31-4 ]
[ 104-88-1 ]
[ 101607-19-6 ]

References: [1]Journal of the Indian Chemical Society,1990,vol. 67,p. 821 - 823.
[2]Patent: US2770619,1954,A .

7
[ 2598-31-4 ]
[ 100-52-7 ]
[ 102060-75-3 ]

References: [1]Pharmazie,1985,vol. 40,p. 307 - 311.
[2]Journal of the Indian Chemical Society,1990,vol. 67,p. 821 - 823.
[3]Acta Chimica Academiae Scientiarum Hungaricae,1955,vol. 6,p. 287,291.
[4]Acta Chimica Academiae Scientiarum Hungaricae,1955,vol. 6,p. 287,291.

8
[ 2598-31-4 ]
5-acetyl-quinoline-7,8-dione-7-oxime [ No CAS ]

References: [1]Journal of the American Chemical Society,1931,vol. 53,p. 1406.

9
[ 2598-31-4 ]
1-(8-benzoyloxy-[5]quinolyl)-ethanone [ No CAS ]

References: [1]Journal of the American Chemical Society,1931,vol. 53,p. 1493,1495.

10
[ 2598-31-4 ]
[ 563-41-7 ]
5-acetylsemicarbazone-8-hydroxyquinoline [ No CAS ]

References: [1]Journal of the Indian Chemical Society,1987,vol. 64,p. 42 - 45.

11
[ 2598-31-4 ]
[ 106-47-8 ]
[ 112519-11-6 ]

References: [1]Journal of the Indian Chemical Society,1987,vol. 64,p. 42 - 45.

12
[ 2598-31-4 ]
[ 123-11-5 ]
[ 101895-45-8 ]

References: [1]Journal of the Indian Chemical Society,1990,vol. 67,p. 821 - 823.
[2]Journal of the Chilean Chemical Society,2012,vol. 57,p. 1287 - 1291.

13
[ 2598-31-4 ]
[ 104-94-9 ]
[ 112519-10-5 ]

References: [1]Journal of the Indian Chemical Society,1987,vol. 64,p. 42 - 45.

14
[ 2598-31-4 ]
[ 75-03-6 ]
5-Acetyl-1-ethyl-8-hydroxy-quinolinium; iodide [ No CAS ]

References: [1]Bulletin of the Chemical Society of Japan,1988,vol. 61,p. 1345 - 1349.

15
[ 2598-31-4 ]
[ 123-72-8 ]
[ 121359-63-5 ]

References: [1]Journal of the Indian Chemical Society,1990,vol. 67,p. 821 - 823.

16
[ 2598-31-4 ]
[ 62-53-3 ]
[ 112519-02-5 ]

References: [1]Journal of the Indian Chemical Society,1987,vol. 64,p. 42 - 45.

17
[ 2598-31-4 ]
[ 105-53-3 ]
[ 118327-28-9 ]

References: [1]Bulletin of the Chemical Society of Japan,1988,vol. 61,p. 1345 - 1349.

18
[ 2598-31-4 ]
[ 99984-66-4 ]

References: [1]Bulletin of the Chemical Society of Japan,1988,vol. 61,p. 4143 - 4146.

19
[ 2598-31-4 ]
C₂₅H₂₀N₄O₄ [ No CAS ]

References: [1]Bulletin of the Chemical Society of Japan,1988,vol. 61,p. 4143 - 4146.

20
[ 2598-31-4 ]
C₂₅H₂₀N₄O₂S₂ [ No CAS ]

References: [1]Bulletin of the Chemical Society of Japan,1988,vol. 61,p. 4143 - 4146.

21
[ 2598-31-4 ]
4-<1-(8-hydroxy-5-quinolinyl)ethylidene>-3,5-pyrazolidinedione [ No CAS ]

References: [1]Bulletin of the Chemical Society of Japan,1988,vol. 61,p. 1345 - 1349.

22
[ 2598-31-4 ]
4-<1-(8-hydroxy-5-quinolinyl)ethylidene>-3,5-isoxazolidinedione [ No CAS ]

References: [1]Bulletin of the Chemical Society of Japan,1988,vol. 61,p. 1345 - 1349.

23
[ 2598-31-4 ]
5-<1-(8-hydroxy-5-quinolinyl)ethylidene>barbituric acid [ No CAS ]

References: [1]Bulletin of the Chemical Society of Japan,1988,vol. 61,p. 1345 - 1349.

24
[ 2598-31-4 ]
5-<1-(8-hydroxy-5-quinolinyl)ethylidene>-2-thiobarbituric acid [ No CAS ]

References: [1]Bulletin of the Chemical Society of Japan,1988,vol. 61,p. 1345 - 1349.

25
[ 2598-31-4 ]
4-<1-(8-hydroxy-5-quinolinyl)ethylidene>-1-phenyl-3,5-pyrazolidinedione [ No CAS ]

References: [1]Bulletin of the Chemical Society of Japan,1988,vol. 61,p. 1345 - 1349.

26
[ 2598-31-4 ]
5-{1-[3,5-Dioxo-isoxazolidin-(4E)-ylidene]-ethyl}-1-ethyl-8-hydroxy-quinolinium; iodide [ No CAS ]

References: [1]Bulletin of the Chemical Society of Japan,1988,vol. 61,p. 1345 - 1349.

27
[ 2598-31-4 ]
5-[1-(3,5-Dioxo-pyrazolidin-4-ylidene)-ethyl]-1-ethyl-8-hydroxy-quinolinium; iodide [ No CAS ]

References: [1]Bulletin of the Chemical Society of Japan,1988,vol. 61,p. 1345 - 1349.

28
[ 2598-31-4 ]
5-(2,2-Bis-ethoxycarbonyl-1-methyl-vinyl)-1-ethyl-8-hydroxy-quinolinium; iodide [ No CAS ]

References: [1]Bulletin of the Chemical Society of Japan,1988,vol. 61,p. 1345 - 1349.

29
[ 2598-31-4 ]
1-Ethyl-8-hydroxy-5-[1-(2,4,6-trioxo-tetrahydro-pyrimidin-5-ylidene)-ethyl]-quinolinium; iodide [ No CAS ]

References: [1]Bulletin of the Chemical Society of Japan,1988,vol. 61,p. 1345 - 1349.

30
[ 2598-31-4 ]
5-[1-(4,6-Dioxo-2-thioxo-tetrahydro-pyrimidin-5-ylidene)-ethyl]-1-ethyl-8-hydroxy-quinolinium; iodide [ No CAS ]

References: [1]Bulletin of the Chemical Society of Japan,1988,vol. 61,p. 1345 - 1349.

31
[ 2598-31-4 ]
5-{1-[3,5-Dioxo-1-phenyl-pyrazolidin-(4E)-ylidene]-ethyl}-1-ethyl-8-hydroxy-quinolinium; iodide [ No CAS ]

References: [1]Bulletin of the Chemical Society of Japan,1988,vol. 61,p. 1345 - 1349.

32
[ 2598-31-4 ]
5-(1,2,3-thiadiazolo)-8-hydroxyquinoline [ No CAS ]

References: [1]Journal of the Indian Chemical Society,1987,vol. 64,p. 42 - 45.

33
[ 2598-31-4 ]
5-(1,2,3-selenadiazolo)-8-hydroxyquinoline [ No CAS ]

References: [1]Journal of the Indian Chemical Society,1987,vol. 64,p. 42 - 45.

34
[ 2598-31-4 ]
2-methyl-2-(8-hydroxyquinolin-5-yl)-3-phenyl-4-thiazolidinone [ No CAS ]

References: [1]Journal of the Indian Chemical Society,1987,vol. 64,p. 42 - 45.

35
[ 2598-31-4 ]
2-methyl-2-(8-hydroxyquinoline-5-yl)-3-(4-chlorophenyl)-4-thiazolidinone [ No CAS ]

References: [1]Journal of the Indian Chemical Society,1987,vol. 64,p. 42 - 45.

36
[ 2598-31-4 ]
2-methyl-2-(8-hydroxyquinoline-5-yl)-3-(4-methoxyphenyl)-4-thiazolidinone [ No CAS ]

References: [1]Journal of the Indian Chemical Society,1987,vol. 64,p. 42 - 45.

37
[ 2598-31-4 ]
1-phenyl-3-chloro-4-methyl-4-(8-chloroacetyloxyquinolin-5-yl)-2-azetidinone [ No CAS ]

References: [1]Journal of the Indian Chemical Society,1987,vol. 64,p. 42 - 45.

Historical Records

Technical Information

• Appel Reaction • Baeyer-Villiger Oxidation • Barbier Coupling Reaction • Baylis-Hillman Reaction • Bucherer-Bergs Reaction • Buchwald-Hartwig C-N Bond and C-O Bond Formation Reactions • Chugaev Reaction • Clemmensen Reduction • Corey-Bakshi-Shibata (CBS) Reduction • Corey-Chaykovsky Reaction • Corey-Kim Oxidation • Dess-Martin Oxidation • Fischer Indole Synthesis • Grignard Reaction • Henry Nitroaldol Reaction • Horner-Wadsworth-Emmons Reaction • Hydride Reductions • Jones Oxidation • Lawesson's Reagent • Leuckart-Wallach Reaction • Martin's Sulfurane Dehydrating Reagent • McMurry Coupling • Meerwein-Ponndorf-Verley Reduction • Mitsunobu Reaction • Moffatt Oxidation • Oxidation of Alcohols by DMSO • Passerini Reaction • Paternò-Büchi Reaction • Petasis Reaction • Peterson Olefination • Pictet-Spengler Tetrahydroisoquinoline Synthesis • Preparation of Alcohols • Preparation of Aldehydes and Ketones • Preparation of Amines • Prins Reaction • Reactions of Alcohols • Reactions of Aldehydes and Ketones • Reactions of Amines • Reactions with Organometallic Reagents • Reformatsky Reaction • Ritter Reaction • Robinson Annulation • Schlosser Modification of the Wittig Reaction • Schmidt Reaction • Sharpless Olefin Synthesis • Specialized Acylation Reagents-Ketenes • Stobbe Condensation • Swern Oxidation • Tebbe Olefination • Ugi Reaction • Wittig Reaction • Wolff-Kishner Reduction

Related Functional Groups of
[ 2598-31-4 ]

Alcohols

A1549290 [N/A]

2,2,2-Trifluoro-1-(3-hydroxyquinolin-6-yl)ethan-1-one

Similarity: 0.94

A410147 [14510-07-7]

8-Hydroxyquinoline-4-carbaldehyde

Similarity: 0.90

A268393 [2598-30-3]

8-Hydroxyquinoline-5-carbaldehyde

Similarity: 0.90

A144078 [N/A]

1-(3-Methoxyquinolin-7-yl)ethan-1-one

Similarity: 0.88

A278868 [57434-87-4]

8-Hydroxyquinoline-5-carbaldehyde hydrochloride

Similarity: 0.88

Ketones

A1549290 [N/A]

2,2,2-Trifluoro-1-(3-hydroxyquinolin-6-yl)ethan-1-one

Similarity: 0.94

A144078 [N/A]

1-(3-Methoxyquinolin-7-yl)ethan-1-one

Similarity: 0.88

A881191 [99973-51-0]

2-Chloro-1-(8-hydroxyquinolin-5-yl)ethanone

Similarity: 0.87

Related Parent Nucleus of
[ 2598-31-4 ]

Quinolines

A1549290 [N/A]

2,2,2-Trifluoro-1-(3-hydroxyquinolin-6-yl)ethan-1-one

Similarity: 0.94

A410147 [14510-07-7]

8-Hydroxyquinoline-4-carbaldehyde

Similarity: 0.90

A268393 [2598-30-3]

8-Hydroxyquinoline-5-carbaldehyde

Similarity: 0.90

A144078 [N/A]

1-(3-Methoxyquinolin-7-yl)ethan-1-one

Similarity: 0.88

A278868 [57434-87-4]

8-Hydroxyquinoline-5-carbaldehyde hydrochloride

Similarity: 0.88

Precautionary Statements-General
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Physical hazards
Code	Phrase
H200	Unstable explosive
H201	Explosive; mass explosion hazard
H202	Explosive; severe projection hazard
H203	Explosive; fire, blast or projection hazard
H204	Fire or projection hazard
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H220	Extremely flammable gas
H221	Flammable gas
H222	Extremely flammable aerosol
H223	Flammable aerosol
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H230	May react explosively even in the absence of air
H231	May react explosively even in the absence of air at elevated pressure and/or temperature
H240	Heating may cause an explosion
H241	Heating may cause a fire or explosion
H242	Heating may cause a fire
H250	Catches fire spontaneously if exposed to air
H251	Self-heating; may catch fire
H252	Self-heating in large quantities; may catch fire
H260	In contact with water releases flammable gases which may ignite spontaneously
H261	In contact with water releases flammable gas
H270	May cause or intensify fire; oxidizer
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H281	Contains refrigerated gas; may cause cryogenic burns or injury
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Health hazards
Code	Phrase
H300	Fatal if swallowed
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H303	May be harmful if swallowed
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H311	Toxic in contact with skin
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H316	Causes mild skin irritation
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H332	Harmful if inhaled
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Environmental hazards
Code	Phrase
H400	Very toxic to aquatic life
H401	Toxic to aquatic life
H402	Harmful to aquatic life
H410	Very toxic to aquatic life with long-lasting effects
H411	Toxic to aquatic life with long-lasting effects
H412	Harmful to aquatic life with long-lasting effects
H413	May cause long-lasting harmful effects to aquatic life
H420	Harms public health and the environment by destroying ozone in the upper atmosphere

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CAS No.: 2598-31-4

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