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[ CAS No. 261763-34-2 ]

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Chemical Structure| 261763-34-2
Chemical Structure| 261763-34-2
Structure of 261763-34-2 * Storage: {[proInfo.prStorage]}

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Alternatived Products of [ 261763-34-2 ]
Alternatived Products of [ 261763-34-2 ]

Product Details of [ 261763-34-2 ]

CAS No. :261763-34-2 MDL No. :MFCD01631333
Formula : C8H6F2O Boiling Point : -
Linear Structure Formula :- InChI Key :N/A
M.W :156.13 g/mol Pubchem ID :-
Synonyms :

Safety of [ 261763-34-2 ]

Signal Word:Warning Class:N/A
Precautionary Statements:P261-P305+P351+P338 UN#:N/A
Hazard Statements:H302-H315-H319-H335 Packing Group:N/A
GHS Pictogram:

Application In Synthesis of [ 261763-34-2 ]

  • Downstream synthetic route of [ 261763-34-2 ]

[ 261763-34-2 ] Synthesis Path-Downstream   1~7

  • 1
  • [ 5292-43-3 ]
  • [ 261763-34-2 ]
  • [ 1422510-63-1 ]
YieldReaction ConditionsOperation in experiment
56% Intermediate 32A. tert-Butyl 3-(2,6-difluoro-3-methylphenyl)-3- hydroxypropanoate: To a suspension of zinc (1.256 g, 19.21 mmol) in dry tetrahydrofuran (18 mL) was added chlorotrimethylsilane (1.228 mL, 9.61 mmol). After 20 min, tert-butyl 2-bromoacetate (1.420 mL, 9.61 mmol) was added. The reaction was stirred at rt for 10 min, then heated at 40 C for 20 min. The reaction mixture was cooled to 0 C under Ar, and <strong>[261763-34-2]2,6-difluoro-3-methylbenzaldehyde</strong> (1.5 g, 9.61 mmol) in 3 mL of dry THF was added. The reaction was allowed to warm to rt and stirred overnight. The reaction mixture was quenched with 5% aqueous NaHC03, filtered, and rinsed with EtOAc. The filtrate was washed with water and brine, dried over MgS04, filtered, concentrated and purified by silica gel chromatography to yield the desired product (1.46 g, 56%). MS (ESI) m/z: 295.1 (M+Na)+
  • 2
  • [ 261763-34-2 ]
  • [ 1422510-64-2 ]
  • 3
  • [ 261763-34-2 ]
  • [ 1422510-62-0 ]
  • 4
  • [ 261763-34-2 ]
  • [ 106-47-8 ]
  • (E)-N-(4-chlorophenyl)-1-(2,6-difluoro-3-methylphenyl)methanimine [ No CAS ]
  • 5
  • [ 261763-34-2 ]
  • 1-(4-chlorophenyl)-5-(2,6-difluoro-3-methylphenyl)-1H-imidazole [ No CAS ]
  • 6
  • [ 261763-34-2 ]
  • [ 1193348-55-8 ]
  • 7
  • [ 261763-34-2 ]
  • 2-chloro-1-(4-chlorophenyl)-5-(2,6-difluoro-3-methylphenyl)-1H-imidazole [ No CAS ]
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