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[ CAS No. 270596-42-4 ]

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Chemical Structure| 270596-42-4
Chemical Structure| 270596-42-4
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Product Details of [ 270596-42-4 ]

CAS No. :270596-42-4 MDL No. :MFCD01318372
Formula : C15H20ClNO4 Boiling Point : 470°C at 760 mmHg
Linear Structure Formula :- InChI Key :N/A
M.W :313.78 g/mol Pubchem ID :2761571
Synonyms :

Safety of [ 270596-42-4 ]

Signal Word:Warning Class:N/A
Precautionary Statements:P261-P305+P351+P338 UN#:N/A
Hazard Statements:H302-H315-H319-H335 Packing Group:N/A
GHS Pictogram:

Application In Synthesis of [ 270596-42-4 ]

  • Upstream synthesis route of [ 270596-42-4 ]
  • Downstream synthetic route of [ 270596-42-4 ]

[ 270596-42-4 ] Synthesis Path-Upstream   1~3

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YieldReaction ConditionsOperation in experiment
96% With sodium hydrogencarbonate In tetrahydrofuran; water at 20℃; for 24 h; Under stirring at room temperature,To a solution of 300 mL of a mixed solvent of 300 mL of tetrahydrofuran and water (vTHF: v H2O = 1: 1)Three reaction bottles,The compound (62.8 g, 0.2 mol, 1 eq) obtained in Example 13, Boc2O (52.4 g, 0.24 mol, 1.2 eq)NaHCO3 (20.2 g, 0.24 mol, 1.2 eq),The reaction was carried out at room temperature for 24h, and the reaction was monitored by TLC.After the reaction is completed,Add 3M dilute hydrochloric acid solution,PH adjusted to 2-3, the aqueous phase was extracted three times with ethyl acetate, the combined organic phase,Dried over anhydrous sodium sulfate,Remove most of the solvent,Recrystallization from ethyl acetate n-hexane to give a white solid in 96percent yield.
Reference: [1] Patent: CN107501112, 2017, A, . Location in patent: Paragraph 0113; 0114; 0115; 0116
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Reference: [1] Patent: CN107501112, 2017, A,
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  • [ 1035695-08-9 ]
  • [ 270596-42-4 ]
Reference: [1] Patent: CN107501112, 2017, A,
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