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[ CAS No. 2766-17-8 ] {[proInfo.proName]}

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Chemical Structure| 2766-17-8
Chemical Structure| 2766-17-8
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Product Details of [ 2766-17-8 ]

CAS No. :2766-17-8 MDL No. :MFCD00056285
Formula : C17H24N2O5 Boiling Point : -
Linear Structure Formula :- InChI Key :-
M.W : 336.38 Pubchem ID :-
Synonyms :

Safety of [ 2766-17-8 ]

Signal Word:Warning Class:N/A
Precautionary Statements:P261-P305+P351+P338 UN#:N/A
Hazard Statements:H302-H315-H319-H335 Packing Group:N/A
GHS Pictogram:

Application In Synthesis of [ 2766-17-8 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 2766-17-8 ]

[ 2766-17-8 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 1149-26-4 ]
  • [ 623-33-6 ]
  • [ 2766-17-8 ]
YieldReaction ConditionsOperation in experiment
99% With 3,3'-(phenylphosphinylidene)bis<2(3H)-benzothiazolone; triethylamine In dichloromethane for 2h; Ambient temperature;
99% With TEA; diphenyl (2,3-dihydro-2-thioxo-3-benzoxazolyl)phosphonate In dichloromethane for 2h; Ambient temperature;
95% With TEA; 1,2-benzisoxazol-3-yl diphenyl phosphate In dichloromethane for 2h; Ambient temperature;
95% With 2,2'-dipyridyl carbonate; triethylamine In dichloromethane at 20℃;
95% With 2,6-dimethylpyridine; 1-[(1-(cyano-​2-​ethoxy-​2-​oxoethylidenaminooxy)​dimethylamino-​morpholino)]-uronium hexafluorophosphate In tetrahydrofuran; water at 20 - 25℃;
94% With triethylamine; 2-Pyridon-1-yl diphenyl phosphate In N,N-dimethyl-formamide for 3h; Ambient temperature;
93% Stage #1: (S)-N-(benzyloxycarbonyl)valine With 1,1'-carbonyldioxydi[2(1H)-pyridone] In dichloromethane at 20℃; Stage #2: glycine ethyl ester hydrochloride With triethylamine In dichloromethane at -18℃;
86% Stage #1: (S)-N-(benzyloxycarbonyl)valine With triethylamine; N,N'-carbonyldisaccharin In dichloromethane at 20℃; for 3h; Stage #2: glycine ethyl ester hydrochloride With triethylamine In dichloromethane at 20℃; for 13h;
86% With chloroformic acid ethyl ester In dichloromethane for 0.166667h; Heating;
With 1-chloro-1-ethoxy-ethene; benzene
With pyridine; 1-(p-chlorobenzenesulfonyloxy)-6-chloro-1,2,3-benzotriazole In dichloromethane
With triethylamine; dicyclohexyl-carbodiimide In dichloromethane
Multistep reaction;
With pyridine; di(1H-benzo[d][1,2,3]triazol-1-yl)carbonate; triethylamine 1.) CH2Cl2, 1 h, 0 deg C, 2.) 3 h, room temp; Yield given. Multistep reaction;
With 3-(5-nitro-2-oxo-1,2-dihydro-1-pyridyl)-1,2-benzisothiazole 1,1,-dioxide; triethylamine 1) dichloromethane, -10 deg C -> 0 deg C, 2 h; 2) dichloromethane, 0 deg C, 2 h, r.t., overnight; Yield given. Multistep reaction;
With triethylamine 1.) CH2Cl2, RT, 30 min; 2.) CH2Cl2, RT, 10 min; Yield given. Multistep reaction;
With pyridine; C15H12N2O3 1.) CH2Cl2, RT, 12 h, 2.) CH2Cl2, RT, 24 h; Yield given. Multistep reaction;
With triethylamine 1.) CH2Cl2, 0 deg C, 20 min, 2.) CH2Cl2, RT, 24 h; Yield given. Multistep reaction;

Reference: [1]Ueda, Mitsuru; Mochizuki, Amane; Hiratsuka, Ichiro; Oikawa, Hideaki [Bulletin of the Chemical Society of Japan, 1985, vol. 58, # 11, p. 3291 - 3297]
[2]Ueda; Mori [Bulletin of the Chemical Society of Japan, 1992, vol. 65, # 6, p. 1636 - 1641]
[3]Ueda, Mitsuru; Oikawa, Hideaki [Journal of Organic Chemistry, 1985, vol. 50, # 6, p. 760 - 763]
[4]Shiina; Suenaga; Nakano; Mukaiyama [Bulletin of the Chemical Society of Japan, 2000, vol. 73, # 12, p. 2811 - 2818]
[5]Cortes-Clerget, Margery; Berthon, Jean-Yves; Krolikiewicz-Renimel, Isabelle; Chaisemartin, Laurent; Lipshutz, Bruce H. [Green Chemistry, 2017, vol. 19, # 18, p. 4263 - 4267]
[6]Kim, Sunggak; Kim, Sung Soo [Journal of the Chemical Society. Chemical communications, 1986, # 9, p. 719]
[7]Shiina, Isamu; Kawakita, Yo-Ichi [Tetrahedron Letters, 2003, vol. 44, # 9, p. 1951 - 1955]
[8]Yadav; Dubey, Suman; Singh, Amrish [Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2003, vol. 42, # 10, p. 2601 - 2603]
[9]Cledera, Pilar; Avendano, Carmen; Carlos Menendez [Journal of Organic Chemistry, 2000, vol. 65, # 6, p. 1743 - 1749]
[10]Heslinga; Arens [Recueil des Travaux Chimiques des Pays-Bas, 1957, vol. 76, p. 982,992]
[11]Itoh,M. et al. [Tetrahedron Letters, 1974, p. 3089 - 3092]
[12]Izdebski,J. et al. [Roczniki Chemii, 1977, vol. 51, p. 81 - 87]
[13]Inomata,K. et al. [Chemistry Letters, 1979, p. 1265 - 1268]
[14]Ueda, Mitsuru; Oikawa, Hideaki; Teshirogi, Takuma [Synthesis, 1983, # 11, p. 908 - 909]
[15]Ahmed, Alauddin; Fukuda, Hirohiko; Inomata, Katsuhiko; Kotake, Hiroshi [Chemistry Letters, 1980, p. 1161 - 1164]
[16]Miyake, Muneharu; Kirisawa, Makoto; Tokutake, Norio [Chemistry Letters, 1985, p. 123 - 126]
[17]Ueda; Oikawa; Kawaharasaki; Imai [Bulletin of the Chemical Society of Japan, 1983, vol. 56, # 8, p. 2485 - 2489]
[18]Orlowska, A.; Izdebski, J. [Polish Journal of Chemistry, 1994, vol. 68, # 4, p. 713 - 718]
  • 2
  • [ 24210-19-3 ]
  • [ 2766-17-8 ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 3 steps 1: hydrazine hydrate / methanol / 1.33 h / Heating 2: p-toluenesulfonic acid / methanol / 16 h / 20 °C 3: 63 percent / Et3N / tetrahydrofuran / 1.33 h / Heating
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