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CAS No. : | 2766-17-8 | MDL No. : | MFCD00056285 |
Formula : | C17H24N2O5 | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | - |
M.W : | 336.38 | Pubchem ID : | - |
Synonyms : |
|
Signal Word: | Warning | Class: | N/A |
Precautionary Statements: | P261-P305+P351+P338 | UN#: | N/A |
Hazard Statements: | H302-H315-H319-H335 | Packing Group: | N/A |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
99% | With 3,3'-(phenylphosphinylidene)bis<2(3H)-benzothiazolone; triethylamine In dichloromethane for 2h; Ambient temperature; | |
99% | With TEA; diphenyl (2,3-dihydro-2-thioxo-3-benzoxazolyl)phosphonate In dichloromethane for 2h; Ambient temperature; | |
95% | With TEA; 1,2-benzisoxazol-3-yl diphenyl phosphate In dichloromethane for 2h; Ambient temperature; |
95% | With 2,2'-dipyridyl carbonate; triethylamine In dichloromethane at 20℃; | |
95% | With 2,6-dimethylpyridine; 1-[(1-(cyano-2-ethoxy-2-oxoethylidenaminooxy)dimethylamino-morpholino)]-uronium hexafluorophosphate In tetrahydrofuran; water at 20 - 25℃; | |
94% | With triethylamine; 2-Pyridon-1-yl diphenyl phosphate In N,N-dimethyl-formamide for 3h; Ambient temperature; | |
93% | Stage #1: (S)-N-(benzyloxycarbonyl)valine With 1,1'-carbonyldioxydi[2(1H)-pyridone] In dichloromethane at 20℃; Stage #2: glycine ethyl ester hydrochloride With triethylamine In dichloromethane at -18℃; | |
86% | Stage #1: (S)-N-(benzyloxycarbonyl)valine With triethylamine; N,N'-carbonyldisaccharin In dichloromethane at 20℃; for 3h; Stage #2: glycine ethyl ester hydrochloride With triethylamine In dichloromethane at 20℃; for 13h; | |
86% | With chloroformic acid ethyl ester In dichloromethane for 0.166667h; Heating; | |
With 1-chloro-1-ethoxy-ethene; benzene | ||
With pyridine; 1-(p-chlorobenzenesulfonyloxy)-6-chloro-1,2,3-benzotriazole In dichloromethane | ||
With triethylamine; dicyclohexyl-carbodiimide In dichloromethane | ||
Multistep reaction; | ||
With pyridine; di(1H-benzo[d][1,2,3]triazol-1-yl)carbonate; triethylamine 1.) CH2Cl2, 1 h, 0 deg C, 2.) 3 h, room temp; Yield given. Multistep reaction; | ||
With 3-(5-nitro-2-oxo-1,2-dihydro-1-pyridyl)-1,2-benzisothiazole 1,1,-dioxide; triethylamine 1) dichloromethane, -10 deg C -> 0 deg C, 2 h; 2) dichloromethane, 0 deg C, 2 h, r.t., overnight; Yield given. Multistep reaction; | ||
With triethylamine 1.) CH2Cl2, RT, 30 min; 2.) CH2Cl2, RT, 10 min; Yield given. Multistep reaction; | ||
With pyridine; C15H12N2O3 1.) CH2Cl2, RT, 12 h, 2.) CH2Cl2, RT, 24 h; Yield given. Multistep reaction; | ||
With triethylamine 1.) CH2Cl2, 0 deg C, 20 min, 2.) CH2Cl2, RT, 24 h; Yield given. Multistep reaction; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
Multi-step reaction with 3 steps 1: hydrazine hydrate / methanol / 1.33 h / Heating 2: p-toluenesulfonic acid / methanol / 16 h / 20 °C 3: 63 percent / Et3N / tetrahydrofuran / 1.33 h / Heating |
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