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Chemical Structure| 29871-85-0 Chemical Structure| 29871-85-0

Structure of 29871-85-0

Chemical Structure| 29871-85-0

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Product Details of [ 29871-85-0 ]

CAS No. :29871-85-0
Formula : C6H7NO2
M.W : 125.13
SMILES Code : O=C1C=C(C2CC2)NO1

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Application In Synthesis of [ 29871-85-0 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 29871-85-0 ]

[ 29871-85-0 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 32249-35-7 ]
  • [ 29871-85-0 ]
YieldReaction ConditionsOperation in experiment
75.2% With hydroxylamine hydrochloride; triethylamine; In methanol; for 2h;Reflux; A solution of <strong>[32249-35-7]methyl 3-cyclopropyl-3-oxopropionate</strong> (4.8 g, 34 mmol) in methanol (80 mL) is mixed with hydroxylamine hydrochloride (2.6 g, 38 mmol) and triethylamine (5.3 mL, 38 mmol), and the mixture is heated under reflux for 2 h. The solvent is distilled out in vacuo. The residue is taken up in EtOAc and filtered through silica gel.Yield: 3.2 g (75.2%).
 

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