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Chemical Structure| 30613-71-9 Chemical Structure| 30613-71-9

Structure of 30613-71-9

Chemical Structure| 30613-71-9

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Product Details of [ 30613-71-9 ]

CAS No. :30613-71-9
Formula : C8H3ClF3NS
M.W : 237.63
SMILES Code : FC(C1=CC=C(N=C=S)C=C1Cl)(F)F
MDL No. :MFCD28667425

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Application In Synthesis of [ 30613-71-9 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 30613-71-9 ]

[ 30613-71-9 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 463-71-8 ]
  • [ 445-13-6 ]
  • [ 30613-71-9 ]
YieldReaction ConditionsOperation in experiment
79% With calcium carbonate; In dichloromethane; water; at 0 - 20℃; under 760.051 Torr;Inert atmosphere; To a suspension of calcium carbonate (1.04 g, 10.4 mmol, Eq: 2.03) and thiophosgene (645 mg, 430 mu, 5.61 mmol, Eq: 1.1) in dichloromethane (13.2 g, 10.0 ml, 155 mmol, Eq: 25.3)/water (10.0 g, 10.0 ml, 555 mmol, Eq: 90.2) at 0, was added 3-chloro-4- (trifluoromethyl)aniline (1 g, 5.11 mmol, Eq: 1.00) The reaction was gradually warmed to room temperature and stirred overnight. Added 10 mL IN HC1. Separated organic layer, dried over sodium sulfate, and chromatographed (60 g Analogix, 100% hex) to give 962 mg (79%) of desired product as colorless oil.
 

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