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Chemical Structure| 320419-47-4 Chemical Structure| 320419-47-4

Structure of 320419-47-4

Chemical Structure| 320419-47-4

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Product Details of [ 320419-47-4 ]

CAS No. :320419-47-4
Formula : C12H11Cl2NO
M.W : 256.13
SMILES Code : O=C1/C(CC2=C1C=C(Cl)C=C2Cl)=C/N(C)C
MDL No. :MFCD00214714

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Application In Synthesis of [ 320419-47-4 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 320419-47-4 ]

[ 320419-47-4 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 52397-81-6 ]
  • [ 4637-24-5 ]
  • [ 320419-47-4 ]
YieldReaction ConditionsOperation in experiment
In tetrahydrofuran; at 83℃; for 3.0h; 202 mg (1 mmol) of <strong>[52397-81-6]4,6-dichloroindan-1-one</strong> are dissolved in 2 ml of tetrahydrofuran, and 263 mg of dimethylformamide dimethyl acetal (2.2 mmol) are added. The solution is stirred at 83 C. for 3 hours and concentrated in vacuo. The residue is triturated with diethyl ether and filtered off with suction. 216 mg of yellow crystals of 4,6-dichloro-2-[1-dimethylaminomethylidene]indan-1-one are obtained.
 

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