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Chemical Structure| 328917-29-9 Chemical Structure| 328917-29-9

Structure of 328917-29-9

Chemical Structure| 328917-29-9

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Product Details of [ 328917-29-9 ]

CAS No. :328917-29-9
Formula : C24H26BO3P
M.W : 404.25
SMILES Code : CC1(C)C(C)(C)OB(C2=CC=CC(P(C3=CC=CC=C3)(C4=CC=CC=C4)=O)=C2)O1
MDL No. :MFCD32206477

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Application In Synthesis of [ 328917-29-9 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 328917-29-9 ]

[ 328917-29-9 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 66127-01-3 ]
  • [ 328917-29-9 ]
  • phen-m-PhDPO [ No CAS ]
YieldReaction ConditionsOperation in experiment
73% With palladium diacetate; potassium carbonate; tricyclohexylphosphine; In ethanol; water; toluene; at 100℃;Inert atmosphere; Under N2 atmosphere,Palladium acetate (17.1mg, 0.08mmol),Tricyclohexylphosphine (42.7mg, 0.15mmol) was added to the compound (3) (2g, 4.95mmol),<strong>[66127-01-3]<strong>[66127-01-3]3-bromo-1,10-phenanthrolin</strong>e</strong> (986mg, 3.806 mmol),Aqueous potassium carbonate solution (2M, 4mL, 8mmol), toluene (50mL), ethanol (8mL) a mixture ofin. The reaction was heated to 100 deg.] C and stirred overnight. After cooling to room temperature, the reaction mixture was poured into water, andExtracted with dichloromethane. The organic layer was dried over anhydrous magnesium sulfate, filtered, and the solvent was removed under reduced pressure by silica gel columnSeparating eluant a mixed solvent of dichloromethane and ethyl acetate, to give a white solid in 73% yield (1.66g)
 

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