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Chemistry
Organic Building Blocks
Nitriles
Dibenzo[b,d]furan-3,7-dicarbonitrile
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[ CAS No. 33763-36-9 ] {[proInfo.proName]}

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Chemical Structure| 33763-36-9
Chemical Structure| 33763-36-9
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Product Details of [ 33763-36-9 ]

CAS No. :33763-36-9 MDL No. :
Formula : C14H6N2O Boiling Point : -
Linear Structure Formula :- InChI Key :-
M.W : 218.21 Pubchem ID :-
Synonyms :

Safety of [ 33763-36-9 ]

Signal Word: Class:
Precautionary Statements: UN#:
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Application In Synthesis of [ 33763-36-9 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 33763-36-9 ]

[ 33763-36-9 ] Synthesis Path-Downstream   1~4

  • 1
  • [ 67019-91-4 ]
  • [ 544-92-3 ]
  • [ 33763-36-9 ]
YieldReaction ConditionsOperation in experiment
97.43% In N,N-dimethyl-formamide for 6h; Heating;
Reference： [1]Wang, Sihe; Hall, James Edwin; Tanious, Farial A.; Wilson, W. David; Patrick, Donald A.; McCurdy, Donald R.; Bender, Brenden C.; Tidwell, Richard R. [European Journal of Medicinal Chemistry, 1999, vol. 34, # 3, p. 215 - 224]
  • 2
  • [ 91371-12-9 ]
  • [ 33763-36-9 ]
Reference： [1]European Journal of Medicinal Chemistry,1999,vol. 34,p. 215 - 224
  • 3
  • [ 67019-91-4 ]
  • [ 33763-36-9 ]
YieldReaction ConditionsOperation in experiment
97.43% With ethylenediamine In ethanol; water; N,N-dimethyl-formamide Results and Discussion 3,7-Dicyano-dibenzofuran 19. A suspension of 3,7-dibromo-dibenzofuran (18, 10.27 g, 31.51 mmol) and copper(I) cyanide (8.23 g, 94.5 mmol) in DMF (80 mL) was refluxed under N2 for 6 h. The reaction mixture was poured into ice-water (300 mL). The precipitated solid was collected and stirred for 5 h in a solution of ethylenediamine (50 mL) in water (300 mL). The solid was filtered off, washed with water, then stirred in 10% sodium cyanide solution (100 mL) for 4 h. The solid was further purified by suspension in hot ethanol (100 mL) to give a pale yellow powder (6.69 g, 97.43%): mp 322-325° C. (dec.); HPLC method 3 tR=16.56 min (96.6 area %); 1H NMR (300 MHz, DMSO-d6) δ 8.51 (d, J=8.3 Hz, 2 H), 8.48 (s, 2 H), 7.95 (dd, J1=8.3 Hz, J2=1.0 Hz, 2 H); EI-MS m/z 218 (M+). Anal. (C14H6N2.0.23H2O) C, H, N.
Reference： [1]Current Patent Assignee: The University of North Carolina at Chapel Hill - US6172104, 2001, B2
  • 4
  • [ 67019-91-4 ]
  • copper(l) cyanide [ No CAS ]
  • [ 33763-36-9 ]
YieldReaction ConditionsOperation in experiment
39% Stage #1: 3,7-dibromodibenzo[b,d]furan; copper(l) cyanide In N,N-dimethyl-formamide at 150℃; for 48h; Inert atmosphere; Stage #2: With hydrogenchloride; iron(III) chloride In water; N,N-dimethyl-formamide for 2h; Inert atmosphere;
Reference： [1]Wu, Shaofei; Liu, Yao; Yu, Guipeng; Guan, Jianguo; Pan, Chunyue; Du, Yong; Xiong, Xiang; Wang, Zhonggang [Macromolecules, 2014, vol. 47, # 9, p. 2875 - 2882]

Tags: 33763-36-9 synthesis path| 33763-36-9 SDS| 33763-36-9 COA| 33763-36-9 purity| 33763-36-9 application| 33763-36-9 NMR| 33763-36-9 COA| 33763-36-9 structure

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