Home Cart Sign in  
Chemical Structure| 3589-41-1 Chemical Structure| 3589-41-1

Structure of Benzyl (cyanomethyl)carbamate
CAS No.: 3589-41-1

Chemical Structure| 3589-41-1

*Storage: {[sel_prStorage]}

*Shipping: {[sel_prShipping]}

,{[proInfo.pro_purity]}

4.5 *For Research Use Only !

{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]} Purity: {[proInfo.pro_purity]}

Change View

Size Price VIP Price

US Stock

Global Stock

In Stock
{[ item.pr_size ]} Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price, item.vip_usd) ]}

US Stock: ship in 0-1 business day
Global Stock: ship in 5-7 days

  • {[ item.pr_size ]}

In Stock

- +

Please Login or Create an Account to: See VIP prices and availability

US Stock: ship in 0-1 business day
Global Stock: ship in 2 weeks

  • 1-2 Day Shipping
  • High Quality
  • Technical Support
Product Citations

Alternative Products

Product Details of [ 3589-41-1 ]

CAS No. :3589-41-1
Formula : C10H10N2O2
M.W : 190.20
SMILES Code : O=C(NCC#N)OCC1=CC=CC=C1
MDL No. :MFCD00033175
InChI Key :DVUXKEFDAGQPQU-UHFFFAOYSA-N
Pubchem ID :244143

Safety of [ 3589-41-1 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302+H312+H332
Precautionary Statements:P280

Application In Synthesis of [ 3589-41-1 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Upstream synthesis route of [ 3589-41-1 ]

[ 3589-41-1 ] Synthesis Path-Upstream   1~2

  • 1
  • [ 64-17-5 ]
  • [ 3589-41-1 ]
  • [ 51030-44-5 ]
YieldReaction ConditionsOperation in experiment
54% at -10 - 20℃; for 3.5 h; (a)
2-benzyloxy-carbonyl-amino-acetimido-ethylester
47.6 g (250 mmol) 2-benzyloxy-carbonyl-amino-acetonitrile in 450 ml of ethanol are combined with 150 ml 5m ethanolic hydrochloric acid at -8° C. with cooling, while keeping the temperature below -5° C.
The mixture is stirred for 1.5 h at -10° C. and for 2 h at ambient temperature.
After evaporation i. vac.
the residue is triturated with diethyl ether, filtered off and dried i. vac.
Yield: 36.60 g (134.2 mmol, 54percent)
C12H16N2O3*HCl (236.29/272.73)
Mass spectrum: (M+H)+=237
References: [1] Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980, p. 2316 - 2321.
[2] Bioorganic and Medicinal Chemistry, 2006, vol. 14, # 9, p. 3185 - 3198.
[3] Patent: US2008/51578, 2008, A1, . Location in patent: Page/Page column 50.
[4] Journal of Medicinal Chemistry, 1982, vol. 25, # 12, p. 1466 - 1473.
[5] Zeitschrift fuer Naturforschung, B: Chemical Sciences, 2001, vol. 56, # 6, p. 547 - 553.
  • 2
  • [ 3589-41-1 ]
  • [ 51030-44-5 ]
References: [1] Ser. chim. 26 <1949> 1, 5, .
 

Historical Records

Technical Information

Categories

Related Functional Groups of
[ 3589-41-1 ]

Aryls

Chemical Structure| 176894-58-9

A929158 [176894-58-9]

(R)-Benzyl (1-cyanoethyl)carbamate

Similarity: 0.91

Chemical Structure| 17343-54-3

A491830 [17343-54-3]

(S)-Benzyl (1-cyanoethyl)carbamate

Similarity: 0.91

Chemical Structure| 65935-09-3

A728502 [65935-09-3]

Benzyl ethylcarbamate

Similarity: 0.91

Chemical Structure| 180976-11-8

A436931 [180976-11-8]

Benzyl (2-(methylamino)ethyl)carbamate

Similarity: 0.87

Chemical Structure| 18807-67-5

A906801 [18807-67-5]

Dibenzyl ethane-1,2-diyldicarbamate

Similarity: 0.87

Amides

Chemical Structure| 176894-58-9

A929158 [176894-58-9]

(R)-Benzyl (1-cyanoethyl)carbamate

Similarity: 0.91

Chemical Structure| 17343-54-3

A491830 [17343-54-3]

(S)-Benzyl (1-cyanoethyl)carbamate

Similarity: 0.91

Chemical Structure| 65935-09-3

A728502 [65935-09-3]

Benzyl ethylcarbamate

Similarity: 0.91

Chemical Structure| 180976-11-8

A436931 [180976-11-8]

Benzyl (2-(methylamino)ethyl)carbamate

Similarity: 0.87

Chemical Structure| 18807-67-5

A906801 [18807-67-5]

Dibenzyl ethane-1,2-diyldicarbamate

Similarity: 0.87

Amines

Chemical Structure| 176894-58-9

A929158 [176894-58-9]

(R)-Benzyl (1-cyanoethyl)carbamate

Similarity: 0.91

Chemical Structure| 17343-54-3

A491830 [17343-54-3]

(S)-Benzyl (1-cyanoethyl)carbamate

Similarity: 0.91

Chemical Structure| 65935-09-3

A728502 [65935-09-3]

Benzyl ethylcarbamate

Similarity: 0.91

Chemical Structure| 180976-11-8

A436931 [180976-11-8]

Benzyl (2-(methylamino)ethyl)carbamate

Similarity: 0.87

Chemical Structure| 18807-67-5

A906801 [18807-67-5]

Dibenzyl ethane-1,2-diyldicarbamate

Similarity: 0.87

Nitriles

Chemical Structure| 176894-58-9

A929158 [176894-58-9]

(R)-Benzyl (1-cyanoethyl)carbamate

Similarity: 0.91

Chemical Structure| 17343-54-3

A491830 [17343-54-3]

(S)-Benzyl (1-cyanoethyl)carbamate

Similarity: 0.91