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Chemical Structure| 36567-87-0 Chemical Structure| 36567-87-0

Structure of 36567-87-0

Chemical Structure| 36567-87-0

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Product Details of [ 36567-87-0 ]

CAS No. :36567-87-0
Formula : C14H9N3O3
M.W : 267.24
SMILES Code : O=C1NC(C2=CC=CC=C2[N+]([O-])=O)=NC3=C1C=CC=C3
MDL No. :N/A

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Application In Synthesis of [ 36567-87-0 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 36567-87-0 ]

[ 36567-87-0 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 5900-59-4 ]
  • [ 36567-87-0 ]
  • 2
  • [ 118-48-9 ]
  • [ 16433-96-8 ]
  • [ 36567-87-0 ]
YieldReaction ConditionsOperation in experiment
82% With copper(l) iodide; ammonium acetate; In neat (no solvent); at 120℃; for 4h; General procedure: A mixture of isatoic anhydride (1.0 mmol), benzonitrile(1.0 mmol), NH4OAc (4.0 mmol), and CuI (0.1 mmol)was heated for 4 h at 120 C. After completion of thereaction as indicated by TLC monitoring, the reactionmixture was cooled to room temperature, and the residuewas purified by column chromatography using n-hexane-EtOAc (4:1) as eluent. The solvent was removed, and thepure product 3a was obtained as a white solid.
 

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