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[ CAS No. 369-30-2 ]

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2D
Chemical Structure| 369-30-2
Chemical Structure| 369-30-2
Structure of 369-30-2 *Storage: {[proInfo.prStorage]}

Quality Control of [ 369-30-2 ]

Related Doc. of [ 369-30-2 ]

SDS
Alternatived Products of [ 369-30-2 ]
Alternatived Products of [ 369-30-2 ]

Product Details of [ 369-30-2 ]

CAS No. :369-30-2MDL No. :MFCD00215839
Formula : C9H9FO3 Boiling Point : 264.2±25.0°C at 760 mmHg
Linear Structure Formula :-InChI Key :-
M.W :184.16Pubchem ID :-
Synonyms :

Computed Properties of [ 369-30-2 ]

TPSA : - H-Bond Acceptor Count : -
XLogP3 : - H-Bond Donor Count : -
SP3 : - Rotatable Bond Count : -

Safety of [ 369-30-2 ]

Signal Word:WarningClass:N/A
Precautionary Statements:P261-P305+P351+P338UN#:N/A
Hazard Statements:H315-H319-H335Packing Group:N/A
GHS Pictogram:

Application In Synthesis of [ 369-30-2 ]

  • Downstream synthetic route of [ 369-30-2 ]

[ 369-30-2 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 350-29-8 ]
  • [ 74-88-4 ]
  • [ 369-30-2 ]
YieldReaction ConditionsOperation in experiment
92% With caesium carbonate; In N,N-dimethyl-formamide; at 20℃; for 4h; STEP 1 : A mixture of <strong>[350-29-8]3-fluoro-4-hydroxybenzoic acid</strong> (500 mg, 3.2 mmol), cesium carbonate (3.1 g, 9.6 mmol) and iodomethane (440 mul, 7.0 mmol) in dimethylformamide (7 mL) was stirred at room temperature for 4 hours. The mixture was diluted with ethyl acetate and washed with 5percent aqueous lithium chloride, IN aqueous sodium hydroxide, brine, then dried over anhydrous sodium sulfate. Filtration and concentration afforded 534 mg, 2.9 mmol (92percent ) of methyl 3-fluoro-4- (methyloxy)benzoate. MS (EI) for C9H9FO3: 185 (MH+).
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