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[ CAS No. 391668-75-0 ]

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2D
Chemical Structure| 391668-75-0
Chemical Structure| 391668-75-0
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Product Details of [ 391668-75-0 ]

CAS No. :391668-75-0MDL No. :MFCD09878908
Formula : C14H17NO3 Boiling Point : -
Linear Structure Formula :-InChI Key :N/A
M.W :247.29Pubchem ID :17852149
Synonyms :

Computed Properties of [ 391668-75-0 ]

TPSA : - H-Bond Acceptor Count : -
XLogP3 : - H-Bond Donor Count : -
SP3 : - Rotatable Bond Count : -

Safety of [ 391668-75-0 ]

Signal Word:WarningClass:N/A
Precautionary Statements:P261-P305+P351+P338UN#:N/A
Hazard Statements:H302-H315-H319-H335Packing Group:N/A
GHS Pictogram:

Application In Synthesis of [ 391668-75-0 ]

  • Upstream synthesis route of [ 391668-75-0 ]
  • Downstream synthetic route of [ 391668-75-0 ]

[ 391668-75-0 ] Synthesis Path-Upstream   1~1

  • 1
  • [ 214614-98-9 ]
  • [ 391668-75-0 ]
YieldReaction ConditionsOperation in experiment
86% With Dess-Martin periodane In dichloromethane at 20℃; for 0.5 h; The above product (163 mg, 0.654 mmol) was dissolved in 3.2 mL of dry dichloromethane, and Dess-Martin periodinane (290 mg, 0.68 mmol) was added to the solution at room temperature.
After the reaction mixture was stirred for 30 min at the same temperature, saturated NaHCO3 aqueous solution was added.
The mixture was extracted with ethyl acetate, and the extract was washed with brine, and dried over MgSO4.
After filtration, the filtrate was concentrated in vacuo and the residue was purified by silica gel column chromatography (hexane/ethyl acetate = 95/5 to 75/25) to obtain the title compound as a white powder (140 mg, 86percent).
Reference: [1] Patent: EP2123637, 2009, A1, . Location in patent: Page/Page column 80
[2] Patent: US2003/232860, 2003, A1, . Location in patent: Page 20
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