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Chemical Structure| 392330-26-6 Chemical Structure| 392330-26-6

Structure of 392330-26-6

Chemical Structure| 392330-26-6

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Product Details of [ 392330-26-6 ]

CAS No. :392330-26-6
Formula : C10H7ClS
M.W : 194.68
SMILES Code : SC1=CC2=CC=C(Cl)C=C2C=C1
MDL No. :MFCD14708202

Safety of [ 392330-26-6 ]

GHS Pictogram:
Signal Word:Danger
Hazard Statements:H301-H314
Precautionary Statements:P501-P270-P264-P280-P303+P361+P353-P301+P330+P331-P363-P301+P310+P330-P304+P340+P310-P305+P351+P338+P310-P405
Class:8(6.1)
UN#:2923
Packing Group:

Application In Synthesis of [ 392330-26-6 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 392330-26-6 ]

[ 392330-26-6 ] Synthesis Path-Downstream   1~2

  • 1
  • 6-Chloronaphthlane-2-sulfonyl Chloride [ No CAS ]
  • [ 102153-63-9 ]
  • [ 392330-26-6 ]
YieldReaction ConditionsOperation in experiment
88% With hydrogenchloride; lithium aluminium tetrahydride; In tetrahydrofuran; ethyl acetate; 1d) 6-Chloro-2-mercaptonaphthalene A solution of 6-chloronaphthalene-2-sulfonyl chloride (20.2 g) obtained in Example 1c) in THF (130 ml) was added dropwise to a solution of LAH (7.07 g) in THF (130 ml) suspension under refluxing, and the mixture was further continued to be refluxed for 1 hour. Ethyl acetate (50 ml) was added dropwise to the reaction mixture and, subsequently, 2N hydrochloric acid (360 ml) was added, and the mixture was extracted with ethyl acetate. The extract was purified by subjecting to silica gel column as it was, to obtain the title compound (13.1 g, 88%). NMR (CDCl3) δ: 3.60 (1H, s), 7.34-7.48 (2H, m), 7.61 (1H, s), 7.66 (1H, s), 7.68-7.81 (2H, m).
  • 2
  • [ 102153-63-9 ]
  • [ 392330-26-6 ]
 

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