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Chemistry
Heterocyclic Building Blocks
Pyridines
1-(3-Methylpyridin-2-yl)thiourea
Chemistry
Heterocyclic Building Blocks
Organic Building Blocks
Pyridines
Amines Amides Thioureas

[ CAS No. 41440-07-7 ] {[proInfo.proName]}

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Chemical Structure| 41440-07-7
Chemical Structure| 41440-07-7
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SDS Specification
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Product Details of [ 41440-07-7 ]

CAS No. :41440-07-7 MDL No. :MFCD03617970
Formula : C7H9N3S Boiling Point : -
Linear Structure Formula :- InChI Key :-
M.W : 167.23 Pubchem ID :-
Synonyms :

Safety of [ 41440-07-7 ]

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Precautionary Statements: UN#:
Hazard Statements: Packing Group:

Application In Synthesis of [ 41440-07-7 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 41440-07-7 ]

[ 41440-07-7 ] Synthesis Path-Downstream   1~4

  • 1
  • [ 51488-85-8 ]
  • [ 41440-07-7 ]
  • [ 79571-62-3 ]
Reference： [1]Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry,1981,vol. 20,p. 683 - 685
  • 2
  • [ 23794-16-3 ]
  • [ 41440-07-7 ]
  • [4-(2-chloro-pyridin-4-yl)-thiazol-2-yl]-(3-methyl-pyridin-2-yl)-amine [ No CAS ]
YieldReaction ConditionsOperation in experiment
82% In ethanol for 6h; Heating;
Reference： [1]Narayana; Vijaya Raj; Ashalatha; Kumari, N. Suchetha [Phosphorus, Sulfur and Silicon and the Related Elements, 2007, vol. 182, # 1, p. 7 - 14]
  • 3
  • [ 17570-98-8 ]
  • [ 41440-07-7 ]
  • N-(3-methylpyridin-2-yl)-4-(pyridin-2-yl)thiazol-2-amine [ No CAS ]
YieldReaction ConditionsOperation in experiment
81% In ethanol; at 80℃; for 5h; Specifically, a mixture of 2-(2-bromoacetyl)pyridine hydrobromide (421 mg, 1.50 mmol) and l-(3-methyl-2-pyridyl)thiourea (251 mg, 1.50 mmol) in ethanol (15 ml) was stirred at 80C for 5h. After cooled to room temperature the mixture was evaporated and the residue was partitioned between AcOEt and 10% aqueous K2CO3. Organic phase was washed with brine, dried over Na2S04 and evaporated. The residue was crystallized from ethanol to give compound 1 (325 mg, 81% yield). XH NMR (300 MHz, DMSO-d6) δ 10.52 (s, 1H), 8.63 - 8.56 (m, 1H), 8.19 (dd, J= 4.8, 1.2 Hz, 1H), 8.05 (d, J= 7.9 Hz, 1H), 7.87 (td, J=7.7, 1.8 Hz, 1H), 7.66 (s, 1H), 7.57 (dd, J= 7.2, 0.6 Hz, 1H), 7.31 (ddd, J= 7.5, 4.8, 1.1 Hz, 1H), 6.92 (dd, J= 7.3, 5.0 Hz, 1H), 2.37 (s, 3H). 13C NMR (75 MHz, DMSO- d6) δ 160.10, 152.56, 150.00, 149.37, 148.83, 143.29, 138.54, 137.05, 122.44, 119.93, 1 19.30, 1 16.37, 109.91, 16.85.
Reference： [1]Patent: WO2014/159938,2014,A1 .Location in patent: Page/Page column 48
  • 4
  • [ 6221-12-1 ]
  • [ 41440-07-7 ]
  • N-(3-methylpyridin-2-yl)-4-(pyridin-3-yl)thiazol-2-amine [ No CAS ]
YieldReaction ConditionsOperation in experiment
37% In ethanol at 80℃; for 2h; Sealed tube; 4.6.1. Procedure 1: general procedure for the synthesis of aminothiazoles and thiazoles (1-18, 22-31, 32-34, 48-50, 52-53) General procedure: A solution of appropriate arylthiourea (1 eq.) or arylthioamide(1 eq.) and aryl-2-bromoethanone (1 eq.) in anhydrous ethanol washeated in a sealed tube at 80 C for 2 h. The progress of reactionwasmonitored by TLC. Ethanol was removed from the reaction mixtureand the resulted residue was washed with aq. NaHCO3. Theaqueous layer was extracted with CH2Cl2 (3 times) and the combinedorganic layer was dried over anhydrous Na2SO4. The filtratewas concentrated in vacuo and the crude product was purified onTeledyne Isco Combiflash Rf purification machine to afford correspondingthiazoles in moderate to good yields.
Reference： [1]Mathew, Bini; Ruiz, Pedro; Dutta, Shilpa; Entrekin, Jordan T.; Zhang, Sixue; Patel, Kaval D.; Simmons, Micah S.; Augelli-Szafran, Corinne E.; Cowell, Rita M.; Suto, Mark J. [European Journal of Medicinal Chemistry, 2021, vol. 210]

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