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Chemical Structure| 425604-49-5 Chemical Structure| 425604-49-5

Structure of 425604-49-5

Chemical Structure| 425604-49-5

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Product Details of [ 425604-49-5 ]

CAS No. :425604-49-5
Formula : C18H30BrN
M.W : 340.34
SMILES Code : CCCCCCN(CCCCCC)C1=CC=C(Br)C=C1
MDL No. :MFCD32706884

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Application In Synthesis of [ 425604-49-5 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 425604-49-5 ]

[ 425604-49-5 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 3839-35-8 ]
  • [ 106-40-1 ]
  • [ 425604-49-5 ]
YieldReaction ConditionsOperation in experiment
81% With tetrabutylammomium bromide; sodium hydroxide; at 100℃; for 8h; Taking paratoluene sulfonic acid hexyl 2.56 g (0.01 µM), at room temperature by adding 0.62 g (0.0036 µM) to bromine, adding 0.05 g ammonium bromide [...] transfer catalyst, heating up to 100 C dropwise 25% sodium hydroxide solution of 1.6 g (0.01 µM), maintaining the temperature reaction 8 h after, to room temperature, extracted with ethyl acetate, dried and filtered, rotary evaporation, to obtain the dark purple viscous liquid, by silica gel column to obtain a pale yellow liquid 0.99 g, N, N - dihexylacrylamide to aniline yield is 81%.
 

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