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Chemical Structure| 453562-01-1 Chemical Structure| 453562-01-1

Structure of 453562-01-1

Chemical Structure| 453562-01-1

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Product Details of [ 453562-01-1 ]

CAS No. :453562-01-1
Formula : C11H15N3O4S
M.W : 285.32
SMILES Code : O=S(N1CCN(C)CC1)(C2=CC=CC([N+]([O-])=O)=C2)=O

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Application In Synthesis of [ 453562-01-1 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 453562-01-1 ]

[ 453562-01-1 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 109-01-3 ]
  • [ 97-08-5 ]
  • [ 453562-01-1 ]
YieldReaction ConditionsOperation in experiment
28 g With triethylamine; In dichloromethane; at -40℃; for 1h; At -40C, to 24g 4-chloro-3-nitrobenzenesulfonyl chloride (CAS109-01-3) in 360ml of methylene chloride was added dropwise 19.6ml triethylamine and 0.4ml 1-methylpiperazine (CAS110-91-8), and stirred at -40C for 1 hour, the temperature was slowly raised to room temperature. Was washed with water and saturated sodium chloride solution, the mixture, with magnesium sulfate and completely concentrated under vacuum. To give 28g as a yellow solid of 1-[(4-chloro-3-nitrophenyl)sulfonyl]-4-methylpiperazine.
 

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