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Organic Light-Emitting Diode (OLED) Materials
1,3-Propylenediphosphonic Acid
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Organic Light-Emitting Diode (OLED) Materials

[ CAS No. 4671-82-3 ] {[proInfo.proName]}

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Cat. No.: {[proInfo.prAm]}
Chemical Structure| 4671-82-3
Chemical Structure| 4671-82-3
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Quality Control of [ 4671-82-3 ]

COA NMR CNMR HPLC LC-MS

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SDS Specification
Alternatived Products of [ 4671-82-3 ]

Product Details of [ 4671-82-3 ]

CAS No. :4671-82-3 MDL No. :MFCD00013960
Formula : C3H10O6P2 Boiling Point : -
Linear Structure Formula :- InChI Key :-
M.W : 204.06 Pubchem ID :-
Synonyms :

Safety of [ 4671-82-3 ]

Signal Word:Warning Class:
Precautionary Statements:P280-P305+P351+P338-P337+P313 UN#:
Hazard Statements:H315-H319-H335 Packing Group:
GHS Pictogram:

Application In Synthesis of [ 4671-82-3 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 4671-82-3 ]

[ 4671-82-3 ] Synthesis Path-Downstream   1~3

  • 1
  • [ 4671-82-3 ]
  • [ CAS Unavailable ]
  • [ 128143-86-2 ]
  • [ CAS Unavailable ]
  • [ CAS Unavailable ]
  • [ CAS Unavailable ]
YieldReaction ConditionsOperation in experiment
95% In water at 200℃; for 48h; High pressure; 6 2.6 Synthesis of [{Cu2(bisterpy)}Mo4F6O9{O3P(CH2)3PO3}] (5) A solution of cupric acetate (0.0451 g, 0.2263 mmol), molybdenum(VI) oxide (0.0872 g, 0.6034 mmol), bisterpy (0.0498 g, 0.1078 mmol), 1,3-propylenediphosphonic acid (0.0548 g, 0.2694 mmol), H2O (10.00 g, 556 mmol), and HF (0.200 mL, 11.49 mmol) with the mole ratio 2.10:5.60:1.00:2.50:5157.70:106.59 was stirred briefly before heating to 200 °C for 48 h with initial and final pH values of 1.5 and 1.0, respectively. Green crystals were isolated in 95% yield that were suitable for X-ray diffraction. IR (KBr pellet, cm-1): 3434(m), 1605(m), 1560(m), 1475(m), 1405(m), 1248(w), 1194(w), 1100(m), 1051(m), 951(m), 924(m), 791(m), 714(w), 612(w), 545(w). Anal. Calc. for Mo4Cu2P2C33H26N6O15F6: C, 27.6; H, 1.81; N, 5.86; F, 7.95. Found: C, 27.2; H, 1.65; N, 5.67; F, 7.44%.
Reference： [1]Jones, Stephanie; Vargas, José M.; Pellizzeri, Steven; O'Connor, Charles J.; Zubieta, Jon [Inorganica Chimica Acta, 2013, vol. 395, p. 44 - 57]
  • 2
  • [ 14389-12-9 ]
  • [ 4671-82-3 ]
  • [ 142-71-2 ]
  • Mo12O40P(3-)*2C6H5N5*3Cu(2+)*12.5H2O*HO(1-)*2C6H4N5(1-) [ No CAS ]
YieldReaction ConditionsOperation in experiment
90% With hydrogen fluoride In water at 100℃; for 96h; 2.5 Synthesis of [Cu3(OH)(4-pyrtet)2(4-Hpyrtet)2(H2O)2][Mo12PO40]·10.5H2O (3·10.5H2O) A solution of cupric acetate (0.138 g, 0.6812 mmol), molybdenum(VI) oxide (0.195 g, 1.3655 mmol), 1,3-propylenediphosphonic acid (0.139 g, 0.7356 mmol), 4-Hpt (0.050 g, 0.3401 mmol), H2O (10.00 g, 556 mmol), and hydrofluoric acid (0.100 mL, 5.79 mmol) with the mole ratio 2.00:4.01:2.16:1.00:1634.81:17.02 was stirred briefly before heating to 100 °C for 4 days (initial and final pH values of 3.0 and 1.0, respectively). Green block crystals suitable for X-ray diffraction were isolated in 90% yield. IR (KBr pellet, cm-1): 3422(s), 1638(s), 1543(s), 1523(m), 1439(m), 1064(s), 959(s), 881(s), 799(s), 745(w). Anal. Calc. for C24H44Cu3Mo12N20O53.50P: C, 10.1; H, 1.55; N, 9.85. Found; C, 9.9; H, 1.44; N, 9.90.
Reference： [1]Jones, Stephanie; Aldous, Amanda; Burkholder, Eric; Zubieta, Jon [Polyhedron, 2013, vol. 52, p. 582 - 590]
  • 3
  • [ 14389-12-9 ]
  • [ 4671-82-3 ]
  • [ 142-71-2 ]
  • Mo12O40P(3-)*C6H6N5(1+)*3Cu(2+)*7.5H2O*HO(1-)*3C6H4N5(1-) [ No CAS ]
YieldReaction ConditionsOperation in experiment
30% In water at 150℃; for 96h; 2.6 Synthesis of [Cu3(OH)(4-pyrtet)3(4-H2pyrtet)(H2O)][Mo12PO40]·7.5H2O (4·7.5H2O) A solution of cupric acetate (0.137 g, 0.6862 mmol), molybdenum(VI) oxide (0.197 g, 1.3689 mmol), 1,3-propylenediphosphonic acid (0.138 g, 0.7304 mmol), 4-Hpt (0.053 g, 0.3605 mmol), and H2O (10.00 g, 556 mmol) with the mole ratio 1.90:3.78:2.03:1.00:1542.30 was stirred briefly before heating to 150 °C for 4 days (initial and final pH values of 3.0 and 1.0, respectively). Green block crystals were isolated in 30% yield. IR (KBr pellet, cm-1): 3422(s), 1638(s), 1543(s), 1524(s), 1437(m), 1203(m), 1063(s), 1016(w), 962(s), 880(s), 805(s), 755(w), 503(w). Anal. Calc. for C24H32Cu3Mo12N20O49.50P: C, 10.4; H, 1.30; N, 10.1. Found: C, 10.2; H, 1.43; N, 10.4%.
Reference： [1]Jones, Stephanie; Aldous, Amanda; Burkholder, Eric; Zubieta, Jon [Polyhedron, 2013, vol. 52, p. 582 - 590]

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