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Chemical Structure| 51818-91-8 Chemical Structure| 51818-91-8

Structure of 51818-91-8

Chemical Structure| 51818-91-8

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Product Details of [ 51818-91-8 ]

CAS No. :51818-91-8
Formula : C13H8O2
M.W : 196.20
SMILES Code : O=CC1=CC=C2C(OC3=CC=CC=C23)=C1
MDL No. :MFCD18451236

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Application In Synthesis of [ 51818-91-8 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 51818-91-8 ]

[ 51818-91-8 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 26608-06-0 ]
  • [ 68-12-2 ]
  • [ 51818-91-8 ]
YieldReaction ConditionsOperation in experiment
Example 12 Dibenzofuran-3-carbaldehyde Combine <strong>[26608-06-0]3-bromodibenzofuran</strong> (0.5 g, 2.0 mmol) and tetrahydrofuran (30 ml). Cool to about -78C. Add a solution of t-butyllithium, 1.6 M solution in hexane (2.2 ml, 3.0 mmol), then warm to about 0C for 10 min. Cool to about -78C and add dimethylformamide (0.5 ml, 5.9 mmol). Warm to room temperature, quench with water, and extract with dichloromethane. Combine the organic layers and wash sequentially with distilled water and brine and then dry (Na2SO4), filter, and concentrate to give a residue. Chromatograph the residue eluting with 8:2 hexane:EtOAc to give the title compound.
 

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