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Chemical Structure| 52694-50-5 Chemical Structure| 52694-50-5

Structure of 52694-50-5

Chemical Structure| 52694-50-5

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Product Details of [ 52694-50-5 ]

CAS No. :52694-50-5
Formula : C7H14ClN
M.W : 147.65
SMILES Code : CN1CC(CCl)CCC1
MDL No. :MFCD00044569

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Application In Synthesis of [ 52694-50-5 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 52694-50-5 ]

[ 52694-50-5 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 7583-53-1 ]
  • [ 75-09-2 ]
  • [ 52694-50-5 ]
YieldReaction ConditionsOperation in experiment
With thionyl chloride; Preparation 1F Following a procedure similar to that described in Preparation 1D above, a solution of 95 g. (0.735 mole) of 3-hydroxymethyl-1-methylpiperidine in 600 ml. of MDC was cooled to 0° C. and treated dropwise with 53.6 ml. of thionyl chloride. When addition was complete, the reaction mixture was heated to reflux for one hour and then taken to dryness to give 135 g. of 3-chloromethyl-1-methylpiperidine.
 

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