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Chemical Structure| 52971-32-1 Chemical Structure| 52971-32-1

Structure of 52971-32-1

Chemical Structure| 52971-32-1

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Product Details of [ 52971-32-1 ]

CAS No. :52971-32-1
Formula : C11H12N2O
M.W : 188.23
SMILES Code : C/C=N/OC1=CN(C)C2=C1C=CC=C2

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Application In Synthesis of [ 52971-32-1 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 52971-32-1 ]

[ 52971-32-1 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 19012-02-3 ]
  • [ 52971-32-1 ]
YieldReaction ConditionsOperation in experiment
With hydroxylamine hydrochloride; In N,N-dimethyl-formamide; at 80℃; for 1h;Inert atmosphere; General procedure: Preparation of Compound Nos. 1, 3, 5, and 42 (0126) One point zero equivalent of the ketone compound 2 obtained in step 1, 1.5 equivalents of hydroxylamine hydrochloride, and double the theoretical amount of dimethylformamide were mixed and stirred while heating in a nitrogen atmosphere at 80 C. for 1 hour. After cooling to room temperature, the reaction mixture was poured into ion-exchanged water for oil-water separation, followed by solvent removal to give an oxime compound 3.
 

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