Home Cart 0 Sign in  

[ CAS No. 5307-02-8 ]

{[proInfo.proName]} ,{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]}
Chemical Structure| 5307-02-8
Chemical Structure| 5307-02-8
Structure of 5307-02-8 * Storage: {[proInfo.prStorage]}

Quality Control of [ 5307-02-8 ]

Related Doc. of [ 5307-02-8 ]

SDS
Alternatived Products of [ 5307-02-8 ]
Alternatived Products of [ 5307-02-8 ]

Product Details of [ 5307-02-8 ]

CAS No. :5307-02-8 MDL No. :MFCD00466319
Formula : C7H10N2O Boiling Point : -
Linear Structure Formula :- InChI Key :N/A
M.W :138.17 g/mol Pubchem ID :21379
Synonyms :

Safety of [ 5307-02-8 ]

Signal Word:Warning Class:N/A
Precautionary Statements:P261-P280-P305+P351+P338 UN#:N/A
Hazard Statements:H302+H312+H332-H315-H319-H335 Packing Group:N/A
GHS Pictogram:

Application In Synthesis of [ 5307-02-8 ]

  • Downstream synthetic route of [ 5307-02-8 ]

[ 5307-02-8 ] Synthesis Path-Downstream   1~15

  • 2
  • [ 5307-02-8 ]
  • [ 501101-53-7 ]
  • 5
  • [ 5307-02-8 ]
  • [ 121-60-8 ]
  • 1,4-bis-[(<i>N</i>-acetyl-sulfanilyl)-amino]-2-methoxy-benzene [ No CAS ]
  • 6
  • [ 97-52-9 ]
  • [ 5307-02-8 ]
YieldReaction ConditionsOperation in experiment
With palladium 10% on activated carbon; hydrazine hydrate; In tetrahydrofuran; at 90℃; for 3.0h; 3.0 g (17.8 mmol) 2-methox.y-4-nitroaniline and 0.8 g palladium on charcoal (10 wt.%) were added to 100 ml tetrahydrofuran (THF). 8.66 mL (1 14 mmol) hydrazine monohydrate in 40 ml THF were cautiously added and the reaction mixture was stirred at 90 C for 3 hours. After cooling, the suspension was filtered and the collected solid washed with THF. The filtrate was reduced to a gray residue under reduced pressure. 2.44 g (17.66 mmol, 99 %) 2- methoxybenzene-l,4-diamine were stored under argon and used without further purification.
  • 7
  • [ 6374-26-1 ]
  • [ 5307-02-8 ]
  • [ 66608-32-0 ]
  • 8
  • [ 5307-02-8 ]
  • [ 90932-86-8 ]
  • 9
  • [ 5307-02-8 ]
  • [ 15945-16-1 ]
  • 10
  • [ 5307-02-8 ]
  • [ 931-59-9 ]
  • C19H16N2OS2 [ No CAS ]
  • 11
  • [ 85-44-9 ]
  • [ 5307-02-8 ]
  • [ 171368-33-5 ]
  • 12
  • [ 66671-82-7 ]
  • [ 5307-02-8 ]
YieldReaction ConditionsOperation in experiment
Nonlimiting examples of suitable aromatic diamines, aminophenols, polyhydric phenols and derivatives thereof, respectively, are the following compounds: ... 2-benzyl-p-phenylenediamine acetate, 2-(4-nitrobenzyl)-p-phenylenediamine, 2-(4-methylphenyl)-p-phenylenediamine, 2-(2,5-diaminophenyl)-5-methylbenzoic acid, 2-methoxy-p-phenylenediamine, 2,3-dimethyl-p-phenylenediamine, 2,5-dimethyl-p-phenylenediamine, 2-methyl-5-methoxy-p-phenylenediamine, ...
Nonlimiting examples of suitable aromatic diamines, aminophenols, polyhydric phenols and derivatives thereof, respectively, are the following compounds: ... 2-benzyl-p-phenylenediamine, 2-(4-nitrobenzyl)-p-phenylenediamine, 2-(4-methylphenyl)-p-phenylenediamine, 2-(2,5-diaminophenyl)-5-methylbenzoic acid, 2-methoxy-p-phenylenediamine, 2,3-dimethyl-p-phenylenediamine, 2,5-dimethyl-p-phenylenediamine, 2-methyl-5-methoxy-p-phenylenediamine, ...
The process of claim 3 wherein said compound of formula (II) is selected from the group consisting of p-phenylenediamine, 2-methyl-p-phenylenediamine, methoxy-para-phenylenediamine, chloro-para-phenylenediamine, 2,6-dimethyl-para-phenylenediamine, 2,5-dimethyl-para-phenylenediamine, 2,3-dimethyl-para-phenylenediamine, 2,6-diethyl-para-phenylenediamine, 2-methyl-5-methoxy-para-phenylenediamine, ...
The process of claim 1 wherein said paraphenylenediamine of formula I is selected from the group consisting of 2-methyl paraphenylenediamine, 2-methoxy paraphenylenediamine, N-methyl-2-chloro paraphenylenediamine, N-furfuryl paraphenylenediamine, 3-methoxy-N'-methyl paraphenylenediamine, 2-chloro paraphenylenediamine, N-methyl paraphenylenediamine, 2,3-dimethylparaphenylenediamine, 5-chloro-N'-methyl paraphenylenediamine, ...
The one-step process of claim 3 wherein said paraphenylenediamine of formula (I) is selected from the group consisting of isopropyl-p-phenylenediamine, p-phenylenediamine, 2-methyl-p-phenylenediamine, methoxy-paraphenylenediamine, chloro-para-phenylenediamine, 2-methyl-5-methoxy-para-phenylenediamine, 2,6-dimethyl-5-methoxy-para-phenylenediamine, N,N-dimethyl-para-phenylenediamine, 3-methyl-4-amino-N,N-diethylaniline, ...
The following compounds with formula (IV) may in particular be cited: paraphenylenediamine, paratoluylenediamine, methoxyparaphenylenediamine, chloroparaphenylenediamine, 2,3-dimethylparaphenylenediamine, 2,6-dimethylparaphenylenediamine, 2,6-diethylparaphenylenediamine, 2,5-dimethylparaphenylenediamine, 2,6-dimethyl 5-methoxyparaphenylenediamine, ...
The method of claim 4 wherein said para-phenylenediamine is selected from the group consisting of p-phenylenediamine, 2-methyl-p-phenylenediamine, methoxy-para-phenylenediamine, chloro-para-phenylenediamine, 2,6-dimethyl-para-phenylenediamine, 2,5-dimethyl-para-phenylenediamine, 2,3-dimethyl-para-phenylenediamine, 2-methyl-5-methoxy-para-phenylenediamine, 2,6-dimethyl-5-methoxy-para-phenyldiamine, ...
methylamine, ... 1,3-diamino-4-ethylbenzene, 1,3-diamino-4-methoxybenzene, 1,3-diamino-4-ethoxybenzene, 1,4-diamino-2-methylbenzene, 1,4-diamino-2-methoxybenzene, 1,4-diamino-2-ethoxybenzene, 1,4-diamino-2-chlorobenzene, 1,4-diamino-2,5-dimethylbenzene, ...
...he aromatic nucleus, for example alkyl groups and halogen atoms. ... 2,4-tolylenediamine 2,4-diaminoanisole 2,4-diaminochlorobenzene 2,5-diaminoanisole 1,2-phenylenediamine 2,6-tolylenediamine 1,4-diaminonaphthalene ...
43 g (79.6% recovery) EXAMPLE 2 Preparation of Tetraethyl-{(2-methoxy-p-phenylene)bis[imino(thiocarbonyl)]diphosphoramidate 2-Methoxy-p-phenylenediamine-H2 SO4 (100 g) is stirred for an hour in a solution containing 42 g of NaOH in 550 ml of H2 O. The diamine is extracted eleven times successively with 200 ml of CH2 Cl2 and the combined extracts are dried over MgSO4. The extract is filtered and evaporated to dryness in vacuo to afford 43 g (79.6% recovery) of 2-methoxy-p-phenylenediamine.
Nonlimiting examples of suitable aromatic diamines, aminophenols, naphthols, polyhydric phenols and derivatives thereof, respectively, are the following compounds: ... 2-benzyl-p-phenylenediamine acetate, 2-(4-nitrobenzyl)-p-phenylenediamine, 2-(4-methylphenyl)-p-phenylenediamine, 2-(2,5-diaminophenyl)-5-methylbenzoic acid, 2-methoxy-p-phenylenediamine, 2,3-dimethyl-p-phenylenediamine, 2,5-dimethyl-p-phenylenediamine, 2-methyl-5-methoxy-p-phenylenediamine, ...

  • 15
  • [ 5307-02-8 ]
  • 2-oxy-benzoic acid sulfinic acid-(5) [ No CAS ]
  • 5-(2,5-diamino-4-methoxy-benzenesulfonyl)-2-hydroxy-benzoic acid [ No CAS ]
Reference: [1]Patent: GB267366,
Historical Records

Related Functional Groups of
[ 5307-02-8 ]

Amines

Chemical Structure| 102-56-7

[ 102-56-7 ]

2,5-Dimethoxyaniline

Similarity: 1.00

Chemical Structure| 116289-67-9

[ 116289-67-9 ]

2-Methoxy-5-phenoxyaniline

Similarity: 0.97

Chemical Structure| 76838-72-7

[ 76838-72-7 ]

5-Methoxy-2-phenoxyaniline

Similarity: 0.97

Chemical Structure| 20734-76-3

[ 20734-76-3 ]

2-Amino-4-methoxyphenol

Similarity: 0.97

Chemical Structure| 6299-67-8

[ 6299-67-8 ]

2,3-Dimethoxyaniline

Similarity: 0.94

Aryls

Chemical Structure| 102-56-7

[ 102-56-7 ]

2,5-Dimethoxyaniline

Similarity: 1.00

Chemical Structure| 116289-67-9

[ 116289-67-9 ]

2-Methoxy-5-phenoxyaniline

Similarity: 0.97

Chemical Structure| 76838-72-7

[ 76838-72-7 ]

5-Methoxy-2-phenoxyaniline

Similarity: 0.97

Chemical Structure| 20734-76-3

[ 20734-76-3 ]

2-Amino-4-methoxyphenol

Similarity: 0.97

Chemical Structure| 6299-67-8

[ 6299-67-8 ]

2,3-Dimethoxyaniline

Similarity: 0.94

Ethers

Chemical Structure| 102-56-7

[ 102-56-7 ]

2,5-Dimethoxyaniline

Similarity: 1.00

Chemical Structure| 116289-67-9

[ 116289-67-9 ]

2-Methoxy-5-phenoxyaniline

Similarity: 0.97

Chemical Structure| 76838-72-7

[ 76838-72-7 ]

5-Methoxy-2-phenoxyaniline

Similarity: 0.97

Chemical Structure| 20734-76-3

[ 20734-76-3 ]

2-Amino-4-methoxyphenol

Similarity: 0.97

Chemical Structure| 6299-67-8

[ 6299-67-8 ]

2,3-Dimethoxyaniline

Similarity: 0.94