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Chemical Structure| 53216-17-4 Chemical Structure| 53216-17-4

Structure of 53216-17-4

Chemical Structure| 53216-17-4

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Product Details of [ 53216-17-4 ]

CAS No. :53216-17-4
Formula : C8H4Cl2O2
M.W : 203.02
SMILES Code : O=CC(C1=C(Cl)C=CC=C1Cl)=O

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Application In Synthesis of [ 53216-17-4 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 53216-17-4 ]

[ 53216-17-4 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 2040-05-3 ]
  • [ 53216-17-4 ]
YieldReaction ConditionsOperation in experiment
With selenium(IV) oxide; In ethanol; water; at 105℃; for 48h;Inert atmosphere; Under nitrogen atmosphere, to a solution of 1-(2,6-dichloropbenyl)ethanone (510 mg, 2.7 mmol) in ethanol (5 mL) and water (0.5 mL), selenium dioxide (330 mg, 3.0 mmol) was added. The reaction mixture was stirred at 105 °C for 48 hours. The solution was filtered on a pad of celite and rinsed with ethanol. The filtrate was concentred to give crude (2,6-dichlorophenyl)(oxo)acetaldehyde which was used without further purification in the next step.
 

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