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[ CAS No. 5382-30-9 ] {[proInfo.proName]}

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Chemical Structure| 5382-30-9
Chemical Structure| 5382-30-9
Structure of 5382-30-9 * Storage: {[proInfo.prStorage]}
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CAS No. :5382-30-9 MDL No. :MFCD03064901
Formula : C9H19NO Boiling Point : -
Linear Structure Formula :- InChI Key :-
M.W : 157.25 Pubchem ID :-
Synonyms :

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* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Upstream synthesis route of [ 5382-30-9 ]
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[ 5382-30-9 ] Synthesis Path-Upstream   1~1

  • 1
  • [ 5382-30-9 ]
  • [ 98-59-9 ]
  • [ 118811-07-7 ]
YieldReaction ConditionsOperation in experiment
51% With pyridine In chloroform at 20℃; [003191 48A. tert-Butyl 4-(tosyloxy)piperidine-1-carboxylate: To an ice cooled solution of tert-butyl-4-hydroxy-piperdine (3.00 g, 14.9 mmol) in CHC13 (30 mL), pyridine (3.6 mL, 45 mmol) and TsC1 (5.68 g, 29.8 mmol) were added and the reactionmixture was stirred at rt overnight. The reaction mixture was diluted with CHC13, washed with 1.5 N aq. HC1 and brine, dried over Na2SO4, and concentrated. Purification via silica chromatography gave 48A (off-white solid, 2.70 g, 7.61 mmol, 51percent yield). LC-MS-Anal. Calc’d for C17H25N05S: 355.15, found [M+Na] 377.9. ‘HNMR(400 MHz, DMSO-d6) ö 7.83 (d, J=7.8 Hz, 2H), 7.49 (d, J=7.8 Hz, 2H), 4.69 (tt, J8.0, 3.8Hz, 1H), 3.49 (ddd, J=13.4, 6.5, 4.1 Hz, 2H), 3.15 (t, J9.4 Hz, 2H), 2.44 (s, 3H), 1.67 -1.75 (m, 2H), 1.45 - 1.54 (m, 2H), 1.38 (s, 9H).
Reference: [1] Patent: WO2014/78609, 2014, A1, . Location in patent: Paragraph 00319
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