Home Cart Sign in  
Chemical Structure| 540473-55-0 Chemical Structure| 540473-55-0

Structure of 540473-55-0

Chemical Structure| 540473-55-0

*Storage: {[sel_prStorage]}

*Shipping: {[sel_prShipping]}

,{[proInfo.pro_purity]}

4.5 *For Research Use Only !

{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]} Purity: {[proInfo.pro_purity]}

Change View

Size Price VIP Price

US Stock

Global Stock

In Stock
{[ item.pr_size ]} Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price, item.vip_usd) ]}

US Stock: ship in 0-1 business day
Global Stock: ship in 5-7 days

  • {[ item.pr_size ]}

In Stock

- +

Please Login or Create an Account to: See VIP prices and availability

US Stock: ship in 0-1 business day
Global Stock: ship in 2 weeks

  • 1-2 Day Shipping
  • High Quality
  • Technical Support
Product Citations

Alternative Products

Product Details of [ 540473-55-0 ]

CAS No. :540473-55-0
Formula : C19H12N2
M.W : 268.31
SMILES Code : N#CC1=CC2=C(C=C1)N(C3=CC=CC=C3)C4=C2C=CC=C4

Safety of [ 540473-55-0 ]

Application In Synthesis of [ 540473-55-0 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 540473-55-0 ]

[ 540473-55-0 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 87220-68-6 ]
  • [ 540473-55-0 ]
YieldReaction ConditionsOperation in experiment
74% With pyridine; hydroxylamine hydrochloride; acetic acid; at 140℃; for 5h; To the reaction mixture were added 3-aldehyde-9-phenyl carbazole (31.4 g, 116 mmol), hydroxylamine hydrochloride (10 g, 140.4 mmol), acetic acid(25.1 g, 418 mmol), pyridine (16.72 g, 209 mmol) 83 mL) are added in this order to the reaction flask, and then the mixture is stirred at 140 DEG C for 5 hours. After the reaction was completed, the reaction mixture was extracted with water and CH 2 Cl 2 , and the obtained organic layer was separated byusing MgSO 4 and column chromatography, and recrystallized from ethanol and hexane to obtain 23 g (74%) of 3-cyano-9 -phenylcarbazole(intermediate B).
 

Historical Records