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Chemical Structure| 55314-30-2 Chemical Structure| 55314-30-2

Structure of 55314-30-2

Chemical Structure| 55314-30-2

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Product Details of [ 55314-30-2 ]

CAS No. :55314-30-2
Formula : C8H9NO2
M.W : 151.16
SMILES Code : O=C(C1=C(C)C=CN=C1C)O
MDL No. :MFCD03265250
InChI Key :XSZKVKMGSAAAJZ-UHFFFAOYSA-N
Pubchem ID :1512561

Safety of [ 55314-30-2 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H315-H319-H335
Precautionary Statements:P261-P305+P351+P338

Application In Synthesis of [ 55314-30-2 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 55314-30-2 ]

[ 55314-30-2 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 37669-78-6 ]
  • [ 55314-30-2 ]
YieldReaction ConditionsOperation in experiment
99% A mixture of <strong>[37669-78-6]ethyl 2,4-dimethylnicotinate</strong> (3.58 g, 20 mmol) and an aqueous solution of NaOH (10M, 20 ml) in ethanol (20 ml) was stirred at room temperature for 24 hours. The mixture was cooled to 0 C. and methanol (200 ml) was added follow by aqueous HCl (10 M) to adjust pH to 7. The resulting precipitated (NaCl) was filtered off.The filtrated was concentrated to remain approximately 20 ml and methanol (100 ml) was added again to precipitate the remaining sodium chloride. The precipitation (NaCl) was repeated until all NaCl was removed from methanolic solution of the reaction mixture. The mixture was concentrated to dryness to yield 1a (3.01 g, 19.9 mmol, 99%).
 

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Related Functional Groups of
[ 55314-30-2 ]

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Related Parent Nucleus of
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