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Chemical Structure| 55970-05-3 Chemical Structure| 55970-05-3

Structure of 55970-05-3

Chemical Structure| 55970-05-3

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Product Details of [ 55970-05-3 ]

CAS No. :55970-05-3
Formula : C14H13N
M.W : 195.26
SMILES Code : CC(N1)=C(C)C2=C1C=CC3=CC=CC=C23
MDL No. :MFCD00850046

Safety of [ 55970-05-3 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H315-H319-H335
Precautionary Statements:P261-P264-P270-P271-P280-P301+P312-P302+P352-P304+P340-P305+P351+P338-P330-P332+P313-P337+P313-P362-P403+P233-P405-P501

Application In Synthesis of [ 55970-05-3 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 55970-05-3 ]

[ 55970-05-3 ] Synthesis Path-Downstream   1~3

  • 1
  • [ 2243-58-5 ]
  • [ 55970-05-3 ]
  • 2
  • [ 2243-58-5 ]
  • [ 78-93-3 ]
  • [ 55970-05-3 ]
YieldReaction ConditionsOperation in experiment
86% With 4-methylbenzenesulfonic acid-based ionic liquid supported on silica gel; In ethanol; at 20℃; for 5h; General procedure: To a solution of phenylhydrazine (10 mmol) and ketone or aldehyde (10 mmol) in ethanol (15 mL) was added catalyst IL-SO3H-SiO2 (1.2 g). The mixture was allowed to stirringat room temperature for a period time specified in Table 2.The reaction was monitored by TLC and GC. After completionof the reaction, the catalyst was recovered by filtration.Evaporation of the solvent under reduced pressuregave the crude product. Further purification was achievedby flash column chromatography on a silica gel to give thedesired product. The recovered catalyst was dried andreused for the next run. Spectroscopic data for selectedproducts is as follows.
  • 3
  • [ 2243-58-5 ]
  • [ 107-87-9 ]
  • [ 55970-05-3 ]
 

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