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CAS No. : | 580-20-1 | MDL No. : | MFCD00016730 |
Formula : | C9H7NO | Boiling Point : | No data available |
Linear Structure Formula : | - | InChI Key : | XCRPPAPDRUBKRJ-UHFFFAOYSA-N |
M.W : | 145.16 | Pubchem ID : | 135426866 |
Synonyms : |
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Signal Word: | Warning | Class: | |
Precautionary Statements: | P261-P280-P305+P351+P338 | UN#: | |
Hazard Statements: | H302-H315-H319-H332-H335 | Packing Group: | |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
70% | With sodium cyanoborohydride; In ethanol; at 20℃; for 4h; | To a solution of 7-hydroxyquinoline (2 g, 13.8 mmol) in 30 mL EtOH is added NaCNBH3 (3.5 g, 55 mmol) in portions. After stirring at room temperature for 4 hr, the mixture is concentrated, extracted with EtOAc, and washed with brine. The organic layer is dried over Na2SO4 and evaporated. The crude product is purified on silica gel using hexane/EtOAc. Yield: 1.44 g (70%). |