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Chemical Structure| 59504-30-2 Chemical Structure| 59504-30-2

Structure of 59504-30-2

Chemical Structure| 59504-30-2

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Product Details of [ 59504-30-2 ]

CAS No. :59504-30-2
Formula : C10H11ClN2O2
M.W : 226.66
SMILES Code : ClC1=CC=CC([N+]([O-])=O)=C1N2CCCC2
MDL No. :MFCD02039776

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Application In Synthesis of [ 59504-30-2 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 59504-30-2 ]

[ 59504-30-2 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 123-75-1 ]
  • [ 2106-49-2 ]
  • [ 59504-30-2 ]
YieldReaction ConditionsOperation in experiment
95.5% With triethylamine; In tetrahydrofuran; at 60℃; Step 1: To a mixture of a (2.0 g, 11.4 mmol, 1.0 eq) and Et3N (2.3 g, 22.8 mmol, 2.0 eq) in THF (40 mL) was added b (1.62 g, 22.8 mmol, 2.0 eq). The reaction mixture was stirred at 60 C overnight, cooled to room temperature, diluted with water (100 mL) and extracted with DCM (50 mL x 2). The extracts were washed with water (20 mL x 2). The organic layer was dried over anhydrous Na2SO4, filtered. The filtrate was concentrated to afford c (2.47 g, 95.5 %). LCMS: 227.1 [M+H]+.
 

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