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Chemical Structure| 5966-51-8 Chemical Structure| 5966-51-8

Structure of 5966-51-8

Chemical Structure| 5966-51-8

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Product Details of [ 5966-51-8 ]

CAS No. :5966-51-8
Formula : C7H18N2O
M.W : 146.23
SMILES Code : OC(CN(C)C)CN(C)C
MDL No. :MFCD00008332

Safety of [ 5966-51-8 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H303-H315-H319-H335
Precautionary Statements:P261-P264-P271-P280-P302+P352-P304+P340+P312-P305+P351+P338-P312-P332+P313-P337+P313-P403+P233-P405-P501

Application In Synthesis of [ 5966-51-8 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 5966-51-8 ]

[ 5966-51-8 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 64-17-5 ]
  • [ 123-47-7 ]
  • [ 75-50-3 ]
  • [ 5966-51-8 ]
  • [ 75-58-1 ]
  • 2
  • [ 5966-51-8 ]
  • [ 74-88-4 ]
  • [ 123-47-7 ]
YieldReaction ConditionsOperation in experiment
21.6 g In dichloromethane; at 0 - 5℃; for 2.0h; (2) 14.6 g (0.1 mol) of 1,3-bis(dimethylamino)-2-propanol and 50 mL of dichloromethane were added to a 250 mL reaction flask, cooled to 0-5 C. with an ice bath, and stirred under stirring. Add 31.2 g (0.22 mol) of methyl iodide dropwise, and continue stirring at 0-5 C. for 2 h after the dropping. An off-white solid gradually formed. Filtration and drying in vacuo gave 28.2 g of off-white solid (crude prodium iodide) with a yield of 65.6%.(3) The crude product was recrystallized with 170 g of ethanol to obtain 21.6 g of the finished product of prodronium iodide. The purity was 97.93% as detected by ion chromatography.
 

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