Home Cart Sign in  
Chemical Structure| 606099-85-8 Chemical Structure| 606099-85-8

Structure of 606099-85-8

Chemical Structure| 606099-85-8

*Storage: {[sel_prStorage]}

*Shipping: {[sel_prShipping]}

,{[proInfo.pro_purity]}

4.5 *For Research Use Only !

{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]} Purity: {[proInfo.pro_purity]}

Change View

Size Price VIP Price

US Stock

Global Stock

In Stock
{[ item.pr_size ]} Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price, item.vip_usd) ]}

US Stock: ship in 0-1 business day
Global Stock: ship in 5-7 days

  • {[ item.pr_size ]}

In Stock

- +

Please Login or Create an Account to: See VIP prices and availability

US Stock: ship in 0-1 business day
Global Stock: ship in 2 weeks

  • 1-2 Day Shipping
  • High Quality
  • Technical Support
Product Citations

Alternative Products

Product Details of [ 606099-85-8 ]

CAS No. :606099-85-8
Formula : C11H7N3O3
M.W : 229.19
SMILES Code : NC1=C(C#N)C(=CO1)C1=CC=C(C=C1)[N+]([O-])=O
MDL No. :MFCD09027186

Safety of [ 606099-85-8 ]

Application In Synthesis of [ 606099-85-8 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 606099-85-8 ]

[ 606099-85-8 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 64611-67-2 ]
  • [ 109-77-3 ]
  • [ 606099-85-8 ]
YieldReaction ConditionsOperation in experiment
80% With diethylamine; In methanol; at 20℃; for 1h; A mixture of Example 13A (5 g, 27.6 mmol) and malononitrile (2.74 g, 41.4 mmol) in methanol (8.6 mL) at room temperature was treated with diethylamine (1.43 mL, 13.8 mmol), stirred for 1 hour, and poured into water. The resulting suspension was filtered and the filter cake was washed with water then purified by flash column chromatography on silica gel with 1:1 ethyl acetate/hexanes to provide 5 g (80%) of the desired product. MS (DCI) m/e 247 (M+NH4)+
  • 2
  • [ 64611-67-2 ]
  • [ 109-89-7 ]
  • [ 109-77-3 ]
  • [ 606099-85-8 ]
YieldReaction ConditionsOperation in experiment
5 g (80%) In methanol; ethyl acetate; EXAMPLE 13B 2-Amino-4-(4-nitrophenyl)-3-furonitrile A mixture of Example 13A (5 g, 27.6 mmol) and malononitrile (2.74 g, 41.4 mmol) in methanol (8.6 mL) at room temperature was treated with diethylamine (1.43 mL, 13.8 mmol), stirred for 1 hour, and poured into water. The resulting suspension was filtered and the filter cake was washed with water then purified by flash column chromatography on silica gel with 1:1 ethyl acetate/hexanes to provide 5 g (80%) of the desired product. MS (DCI) m/e 247 (M+NH4)+.
 

Historical Records

Technical Information

Categories