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Chemical Structure| 60903-84-6 Chemical Structure| 60903-84-6

Structure of 60903-84-6

Chemical Structure| 60903-84-6

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Product Details of [ 60903-84-6 ]

CAS No. :60903-84-6
Formula : C8H5ClF4
M.W : 212.57
SMILES Code : CC1=C(F)C(F)=C(C(F)=C1F)CCl
MDL No. :MFCD09263726

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Application In Synthesis of [ 60903-84-6 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 60903-84-6 ]

[ 60903-84-6 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 79538-03-7 ]
  • [ 60903-84-6 ]
YieldReaction ConditionsOperation in experiment
95% With thionyl chloride; N,N-dimethyl-formamide; In dichloromethane; at 0℃; (1) 190g of 4-methyltetrafluorobenzyl alcohol and 1500mL of dry dichloromethane was placed in a two-necked flask at a temperature below 0 cooling reaction,And dropping 20 to 50 drops of DMF catalyzed and uniformly stirred,After that, 125 g of thionyl chloride was added dropwise at a dropping rate of 25 g / h,And two bottles of the original solution reaction,And through the TLC plate detection of raw material reaction is completed,The reaction formula is; (2) the mixed solution in step (1) was stirred for 1 hour and then concentrated by a rotary evaporator under reduced pressure,After cooling 10 ~ 30min was added petroleum ether and stirred,Filtered and dried at 50 C to give 195.5 g of 4-methyltetrafluorobenzyl chloride as a white powdery solid,The yield is 95%
 

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