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[ CAS No. 60933-65-5 ] {[proInfo.proName]}

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Cat. No.: {[proInfo.prAm]}
Chemical Structure| 60933-65-5
Chemical Structure| 60933-65-5
Structure of 60933-65-5 * Storage: {[proInfo.prStorage]}
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Product Details of [ 60933-65-5 ]

CAS No. :60933-65-5 MDL No. :MFCD00151460
Formula : C7H9NOS Boiling Point : -
Linear Structure Formula :- InChI Key :-
M.W : 155.22 Pubchem ID :-
Synonyms :

Safety of [ 60933-65-5 ]

Signal Word:Warning Class:N/A
Precautionary Statements:P264-P270-P301+P312-P330-P501 UN#:N/A
Hazard Statements:H302 Packing Group:N/A
GHS Pictogram:

Application In Synthesis of [ 60933-65-5 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 60933-65-5 ]

[ 60933-65-5 ] Synthesis Path-Downstream   1~9

  • 1
  • [ 939-80-0 ]
  • [ 60933-65-5 ]
  • C14H11N3O3S [ No CAS ]
  • 2
  • [ 34052-37-4 ]
  • [ 60933-65-5 ]
  • C20H16N2O4S [ No CAS ]
YieldReaction ConditionsOperation in experiment
90% With caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl In toluene at 135℃; for 3h; microwave irradiation;
  • 3
  • [ 14920-87-7 ]
  • [ 60933-65-5 ]
  • C15H16NSO3Cl [ No CAS ]
YieldReaction ConditionsOperation in experiment
92% Stage #1: 2,6-dichlorobenzoic acid methyl ester; (R)-S-methyl-S-phenylsulfoximine With caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl In toluene at 20℃; for 0.5h; Stage #2: In toluene at 135℃; for 1.5h; microwave irradiation; Further stages.;
  • 4
  • [ 60933-65-5 ]
  • [ 82-46-2 ]
  • C21H14NSO3Cl [ No CAS ]
  • 5
  • [ 320-60-5 ]
  • [ 60933-65-5 ]
  • C14H11NSOClF3 [ No CAS ]
  • 6
  • [ 328-84-7 ]
  • [ 60933-65-5 ]
  • C14H11NSOClF3 [ No CAS ]
  • C14H11NSOClF3 [ No CAS ]
  • 7
  • [ 65340-70-7 ]
  • [ 60933-65-5 ]
  • [ 1085526-24-4 ]
YieldReaction ConditionsOperation in experiment
73% With 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene; sodium t-butanolate;tris-(dibenzylideneacetone)dipalladium(0); In 1,4-dioxane; at 110℃; Intermediate 10: Preparation of 4-chloro-6-[methyl(oxido)phenyl-lambda4- sulphanylidene]amino}quinoline960 mg (6.19 mmol) of R-(-)-S-methyl-S-phenylsulphoximine, 142 mg (0.16 mmol) of tris(dibenzylideneacetone)dipalladium, 215 mg (0.37 mmol) of 9,9-dimethyl-4,5-bis(diphenylphosphino)xanthene and 543 mg (7.42 mmol) of sodium tert-butoxide are added to 1.5 g (6.19 mmol) of 6-bromo-4- chloroquinoline in 64 ml of 1,4-dioxane under argon. After stirring at 1100C overnight, the mixture is cooled and filtered through Celite. The solvent is removed from the filtrate under reduced pressure, and the residue is purified by chromatography on a silica gel column (mobile phase: dichloromethane: methanol 100:1 ). 1.43 g (73%) of the title compound are obtained.1H-NMR (500 MHz, D6-DMSO): delta = 3.52 (s, 3H), 7.4-7.46 (m, 2H), 7.53-7.7 (m, 4H), 7.86 (d, 1H), 8.0 (d, 2H), 8.56 (d, 1 H). MS (ESpos): 317.1 [M+H]
  • 8
  • [ 886501-12-8 ]
  • [ 60933-65-5 ]
  • (R)-7-piperidinyl-2,1-benzothiazine [ No CAS ]
YieldReaction ConditionsOperation in experiment
82% With tris-(dibenzylideneacetone)dipalladium(0); caesium carbonate; ruphos In toluene at 135℃; for 36h;
  • 9
  • [ 886501-36-6 ]
  • [ 60933-65-5 ]
  • (R)-7-morpholino-2,1-benzothiazine [ No CAS ]
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