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Chemical Structure| 6195-54-6 Chemical Structure| 6195-54-6

Structure of 6195-54-6

Chemical Structure| 6195-54-6

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Product Details of [ 6195-54-6 ]

CAS No. :6195-54-6
Formula : C44H48O23
M.W : 944.84
SMILES Code : O=C1C=C(C2=CC=C(OC)C(OC(C)=O)=C2)OC3=CC(O[C@H]4[C@@H]([C@H]([C@@H]([C@@H](CO[C@H]5[C@@H]([C@@H]([C@H]([C@H](C)O5)OC(C)=O)OC(C)=O)OC(C)=O)O4)OC(C)=O)OC(C)=O)OC(C)=O)=CC(OC(C)=O)=C13

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Application In Synthesis of [ 6195-54-6 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 6195-54-6 ]

[ 6195-54-6 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 108-24-7 ]
  • [ 520-27-4 ]
  • [ 6195-54-6 ]
YieldReaction ConditionsOperation in experiment
62% With sodium fluoride; at 130℃; for 0.583333h;Microwave irradiation; Diosmin (2, 0.05 g, 0.08 mmol) and NaF (0.42 g, 10 mmol) were mixed in acetic anhydride (4 mL) and the mixture was kept under MW irradiation (400 W) at 130 C, for 35 min. After cooling, the solution obtained was poured into ice and then extracted with CH2Cl2. The organic layer was extracted with NaHCO3 followed by crystallization from MeOH/H2O provided 5,3-O-acetyl-2-(3-O-acetyl-4-methoxyphenyl)-7-[2,3,4-tri-O-acetyl-alpha-L-rhamnopyranosyl-(16)-2,3,4-tri-O-acetyl-beta-D-glucopyranosyloxy] oxychromen-4-one (6) as a yellow solid (0.048 g, 0.051 mmol, 62 % yield); mp 135-138 C.
  • 2
  • [ 520-26-3 ]
  • [ 6195-54-6 ]
 

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