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Chemical Structure| 623-30-3 Chemical Structure| 623-30-3

Structure of 623-30-3

Chemical Structure| 623-30-3

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Product Details of [ 623-30-3 ]

CAS No. :623-30-3
Formula : C7H6O2
M.W : 122.12
SMILES Code : O=C/C=C/C1=CC=CO1
MDL No. :MFCD00003256
InChI Key :VZIRCHXYMBFNFD-HNQUOIGGSA-N
Pubchem ID :1549521

Safety of [ 623-30-3 ]

GHS Pictogram:
Signal Word:Danger
Hazard Statements:H302+H312+H332-H314
Precautionary Statements:P260-P280-P303+P361+P353-P301+P330+P331-P304+P340+P310-P305+P351+P338+P310
Class:8
UN#:1759
Packing Group:

Application In Synthesis of [ 623-30-3 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 623-30-3 ]

[ 623-30-3 ] Synthesis Path-Downstream   1~5

  • 1
  • [ 623-30-3 ]
  • [ 6281-32-9 ]
  • C17H15NO3 [ No CAS ]
  • C17H15NO3 [ No CAS ]
  • C17H15NO3 [ No CAS ]
  • C17H15NO3 [ No CAS ]
  • 2
  • [ 98-01-1 ]
  • [ 64-17-5 ]
  • [ 623-30-3 ]
  • [ 13529-27-6 ]
  • [ 614-99-3 ]
YieldReaction ConditionsOperation in experiment
With oxygen; potassium carbonate; at 140℃; under 2250.23 Torr; for 4h;Autoclave; Sealed tube; General procedure: Catalytic experiments were carried out in a 120 mL autoclaveequipped with a magnetic stirrer and automatic temperature control.After the FUR, Au catalyst, K2CO3 and the alcohol were added,the reactor was sealed, and purged with pure O2 for three times toremove the air. Then, the pressure of oxygen was charged to 0.3MPa and the reaction mixture was heated to 140 C and kept for4 h. When the reaction was finished, the solution was diluted withacetonitrile after the reactor was cooled to room temperature. Theproducts were qualitatively detected by an Agilent 7890A/5975Cgas chromatography-mass spectrometry (GC-MS). The conversionof FUR and selectivity of the product were quantitatively obtainedby GC instrument with the FID detector.
  • 3
  • [ 98-01-1 ]
  • [ 64-17-5 ]
  • [ 98-00-0 ]
  • [ 623-30-3 ]
  • [ 13529-27-6 ]
  • [ 614-99-3 ]
YieldReaction ConditionsOperation in experiment
With oxygen; potassium carbonate; calcium oxide; at 140℃; under 2250.23 Torr; for 4h;Autoclave; Sealed tube; General procedure: Catalytic experiments were carried out in a 120 mL autoclaveequipped with a magnetic stirrer and automatic temperature control.After the FUR, Au catalyst, K2CO3 and the alcohol were added,the reactor was sealed, and purged with pure O2 for three times toremove the air. Then, the pressure of oxygen was charged to 0.3MPa and the reaction mixture was heated to 140 C and kept for4 h. When the reaction was finished, the solution was diluted withacetonitrile after the reactor was cooled to room temperature. Theproducts were qualitatively detected by an Agilent 7890A/5975Cgas chromatography-mass spectrometry (GC-MS). The conversionof FUR and selectivity of the product were quantitatively obtainedby GC instrument with the FID detector.
  • 4
  • [ 98-01-1 ]
  • [ 64-17-5 ]
  • [ 623-30-3 ]
  • [ 13529-27-6 ]
  • 5
  • [ 98-01-1 ]
  • [ 64-17-5 ]
  • [ 98-00-0 ]
  • [ 623-30-3 ]
  • [ 13529-27-6 ]
 

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Technical Information

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