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CAS No. : | 62584-23-0 | MDL No. : | MFCD04115832 |
Formula : | C8H5ClF3NO | Boiling Point : | 258°C at 760 mmHg |
Linear Structure Formula : | - | InChI Key : | - |
M.W : | 223.58 | Pubchem ID : | 3770849 |
Synonyms : |
|
TPSA :Topological Polar Surface Area | 43.1 | H-Bond Acceptor Count : | 4 |
XLogP3 : | - | H-Bond Donor Count : | 1 |
SP3 : | 0.13 | Rotatable Bond Count : | 1 |
Signal Word: | Warning | Class: | N/A |
Precautionary Statements: | P261-P305+P351+P338 | UN#: | N/A |
Hazard Statements: | H302-H315-H319-H335 | Packing Group: | N/A |
GHS Pictogram: |
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Yield | Reaction Conditions | Operation in experiment |
---|---|---|
In dichloromethane; at 40.0℃; | General procedure: Oxalyl chloride (6.61mmol) was added dropwise into a stirred solution of the appropriate benzamide (2.6mmol) in CH2Cl2 (10mL). The mixtures were heated at reflux for 20-22h. Then, solvents were evaporated in vacuo to give the respective crude benzoyl isocyanates 4a-k, which were used immediately in the next step without purification. Aminoindolin-2-one (2.8mmol) was added into a stirred solution of the appropriate benzoyl isocyanate (2.8mmol) in acetonitrile (10mL). After addition, each mixture was heated at 70-80C for 2-3h. The solid products were each filtered, washed with acetonitrile, and air dried. |
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