Home Cart Sign in  
Chemical Structure| 6324-72-7 Chemical Structure| 6324-72-7

Structure of 6324-72-7

Chemical Structure| 6324-72-7

*Storage: {[sel_prStorage]}

*Shipping: {[sel_prShipping]}

,{[proInfo.pro_purity]}

4.5 *For Research Use Only !

{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]} Purity: {[proInfo.pro_purity]}

Change View

Size Price VIP Price

US Stock

Global Stock

In Stock
{[ item.pr_size ]} Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price, item.vip_usd) ]}

US Stock: ship in 0-1 business day
Global Stock: ship in 5-7 days

  • {[ item.pr_size ]}

In Stock

- +

Please Login or Create an Account to: See VIP prices and availability

US Stock: ship in 0-1 business day
Global Stock: ship in 2 weeks

  • 1-2 Day Shipping
  • High Quality
  • Technical Support
Product Citations

Alternative Products

Product Details of [ 6324-72-7 ]

CAS No. :6324-72-7
Formula : C5H5N5OS
M.W : 183.19
SMILES Code : NC(NC1=C2NC(N1)=S)=NC2=O
MDL No. :MFCD00075623
InChI Key :JHEKNTQSGTVPAO-UHFFFAOYSA-N
Pubchem ID :135423614

Safety of [ 6324-72-7 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H315-H319-H335
Precautionary Statements:P261-P280-P301+P312-P302+P352-P305+P351+P338

Application In Synthesis of [ 6324-72-7 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 6324-72-7 ]

[ 6324-72-7 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 6324-72-7 ]
  • [ 51012-64-7 ]
  • [ 1595278-58-2 ]
YieldReaction ConditionsOperation in experiment
46.6% With sodium hydroxide; In water; at 20℃; for 1h; General procedure: In a round bottom flask equipped with a stir bar was dissolved 2-amino-6-hydroxy-8-mercaptopurine (1-2 mmol, 1.0 equiv) in aqueous sodium hydroxide (0.4 N, 10 mL) and corresponding phenyl substituted 2-bromoacetophenones (1.25-2.5 mmol,1.25 equiv) dissolved in EtOH (2 mL) was added. The mixtures were stirred for 1 h at room temperature before the solution was neutralized by drop wise addition of HCl (1 N) to yield aprecipitate. The precipitate was collected via vacuum filtration,washed with diethyl ether and verified to be pure via LC-MS and1H NMR.
  • 2
  • [ 40299-87-4 ]
  • [ 6324-72-7 ]
  • [ 486408-79-1 ]
YieldReaction ConditionsOperation in experiment
43% With sodium hydroxide; In water; at 20℃; for 1h; General procedure: In a round bottom flask equipped with a stir bar was dissolved 2-amino-6-hydroxy-8-mercaptopurine (1-2 mmol, 1.0 equiv) in aqueous sodium hydroxide (0.4 N, 10 mL) and corresponding phenyl substituted 2-bromoacetophenones (1.25-2.5 mmol,1.25 equiv) dissolved in EtOH (2 mL) was added. The mixtures were stirred for 1 h at room temperature before the solution was neutralized by drop wise addition of HCl (1 N) to yield aprecipitate. The precipitate was collected via vacuum filtration,washed with diethyl ether and verified to be pure via LC-MS and1H NMR.
 

Historical Records

Technical Information

Categories