Home Cart Sign in  
Chemical Structure| 65764-49-0 Chemical Structure| 65764-49-0

Structure of 65764-49-0

Chemical Structure| 65764-49-0

*Storage: {[sel_prStorage]}

*Shipping: {[sel_prShipping]}

,{[proInfo.pro_purity]}

4.5 *For Research Use Only !

{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]} Purity: {[proInfo.pro_purity]}

Change View

Size Price VIP Price

US Stock

Global Stock

In Stock
{[ item.pr_size ]} Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price, item.vip_usd) ]}

US Stock: ship in 0-1 business day
Global Stock: ship in 5-7 days

  • {[ item.pr_size ]}

In Stock

- +

Please Login or Create an Account to: See VIP prices and availability

US Stock: ship in 0-1 business day
Global Stock: ship in 2 weeks

  • 1-2 Day Shipping
  • High Quality
  • Technical Support
Product Citations

Alternative Products

Product Details of [ 65764-49-0 ]

CAS No. :65764-49-0
Formula : C16H21NO3
M.W : 275.34
SMILES Code : O=C1N(OCCCCCCCC)C(C2=C1C=CC=C2)=O
MDL No. :MFCD01407878

Safety of [ 65764-49-0 ]

Application In Synthesis of [ 65764-49-0 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 65764-49-0 ]

[ 65764-49-0 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 524-38-9 ]
  • [ 3386-35-4 ]
  • [ 6674-22-2 ]
  • [ 65764-49-0 ]
YieldReaction ConditionsOperation in experiment
9.40 g (98%) With sodium hydrogencarbonate; In ethyl acetate; N,N-dimethyl-formamide; a) Synthesis of 2-(octyloxy)-1H-isoindole-1,3(2H)-dione A solution of 2-hydroxy-1,3-isoindoledione (5.76 g, 35.2 mmol), octyl 4-methylbenzenesulfonate (10.00 g, 35.2 mmol) and 1,8-diazabicyclo[5.4.0]undec-7-ene (DBU, 5.35 g, 35.2 mmol) in DMF (300 ml) was heated at 80 C. for 17 h. The color of the reaction mixture turned from dark brown to clear yellow. The reaction mixture was concentrated, taken up in ethyl acetate, washed with a saturated solution of NaHCO3 (3*) until the organic phase became colorless. Drying (Na2SO4) and concentrating gave 9.40 g (98%) of a yellow oil that slowly crystallizes. 1H-NMR (CDCl3): 7.88-7.81 (m, 2H); 7.79-7.71 (m, 2H); 4.20 (t, J=6.9, 2H); 1.85-1.74 (m, 2H); 1.54-1.42 (m, 2H); 1.41-1.20 (m, 8H); 0.88 (t, J=6.9, 3H). 13C-NMR (CDCl3): 163.69 (s); 134.42 (d); 129.02 (s); 123.48 (d); 78.66 (t); 31.78 (t); 29.29 (t); 29.16 (t); 28.17 (t); 25.56 (t); 22.65 (t); 14.09 (q).
 

Historical Records