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Chemical Structure| 69797-47-3 Chemical Structure| 69797-47-3

Structure of 69797-47-3

Chemical Structure| 69797-47-3

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Product Details of [ 69797-47-3 ]

CAS No. :69797-47-3
Formula : C11H11FO3
M.W : 210.20
SMILES Code : O=C(OC)CCC(C1=CC=CC(F)=C1)=O
MDL No. :MFCD11617549

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Application In Synthesis of [ 69797-47-3 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 69797-47-3 ]

[ 69797-47-3 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 69797-47-3 ]
  • [ 703-67-3 ]
YieldReaction ConditionsOperation in experiment
53.97% With methanesulfonic acid; phosphorus pentoxide; A solution of methanesulfonic acid (75 mL) and P2O5 was stirred at 85 ° C for 15 minutes, at which point most of the P2Os had dissolved. An additional 15 mL of methanesulfonic acid was added dropwise, and the mixture was stirred at 85 ° C for 2 hours. The reaction mixture was poiured into 500 mL of water and extracted twice with 400 mL of EtOAc. The combined organic layers were washed with saturated NaHCOs, water, and saturated brine, and then dried over MgSO4. The solvent was removed under reduced pressure to give an oil that was eluted through silica gel using hexanes/EtOAc (9:1). Removal of solvent under reduced pressure yielded 6.06 g, 36.91 mmol, 53.97percent) of 6-nuoro-3,4-dihydro-2H-naphthalen-l-one as a yellow oil. MS: 165 (M+H)+.
 

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