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Chemical Structure| 7033-51-4 Chemical Structure| 7033-51-4

Structure of 7033-51-4

Chemical Structure| 7033-51-4

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Product Details of [ 7033-51-4 ]

CAS No. :7033-51-4
Formula : C14H8ClNO2
M.W : 257.67
SMILES Code : O=C1OC(C2=CC=CC=C2)=NC3=CC=C(Cl)C=C13
MDL No. :MFCD00640544

Safety of [ 7033-51-4 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H315-H319-H335
Precautionary Statements:P261-P264-P271-P280-P302+P352-P304+P340-P305+P351+P338-P312-P362-P403+P233-P501

Application In Synthesis of [ 7033-51-4 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 7033-51-4 ]

[ 7033-51-4 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 13421-00-6 ]
  • [ 100-47-0 ]
  • [ 7033-51-4 ]
YieldReaction ConditionsOperation in experiment
80% With 1-butyl-3-methylimidazolium hydroxide; In neat (no solvent); for 5h;Green chemistry; General procedure: A mixture of benzonitrile(2.0 mmol) and o-iodo<strong>[13421-00-6]benzoic acid</strong> (2.0 mmol) and [bmIm]OH (35mol) was stirred at room temperature for (3-5) h. After completion of reaction as indicated byTLC, 20mL of water was added to the reaction mixture and stirred well. The product was extracted with ether (3×20 mL). The combined organic layers were dried over anhydrous Na2SO4 to afford the crude product, this crude product was taken to column in order to obtain analytically pure compound 4(a-m)(77-91%). After isolation of the product, the remaining aqueous layer containing the ionic liquid was washed with ether (2x10mL) to remove organic impurity and filtered. The filtrate was extracted with dichloromethane(2×10mL), dried over MgSO4 and evaporated under reduced pressure to afford [bmIm]OH, which was reused five times in subsequent runs without further purification.
 

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