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[ CAS No. 7328-91-8 ] {[proInfo.proName]}

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Chemical Structure| 7328-91-8
Chemical Structure| 7328-91-8
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Product Details of [ 7328-91-8 ]

CAS No. :7328-91-8 MDL No. :MFCD00009801
Formula : C5H14N2 Boiling Point : -
Linear Structure Formula :C(CH3)2(CH2NH2)2 InChI Key :DDHUNHGZUHZNKB-UHFFFAOYSA-N
M.W : 102.18 Pubchem ID :81770
Synonyms :

Safety of [ 7328-91-8 ]

Signal Word:Danger Class:8,3
Precautionary Statements:P280-P305+P351+P338-P310 UN#:2920
Hazard Statements:H226-H314 Packing Group:
GHS Pictogram:

Application In Synthesis of [ 7328-91-8 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Upstream synthesis route of [ 7328-91-8 ]
  • Downstream synthetic route of [ 7328-91-8 ]

[ 7328-91-8 ] Synthesis Path-Upstream   1~15

  • 1
  • [ 126-30-7 ]
  • [ 26734-09-8 ]
  • [ 7328-91-8 ]
Reference: [1] Angewandte Chemie - International Edition, 1999, vol. 38, # 3, p. 351 - 354
  • 2
  • [ 762-98-1 ]
  • [ 7328-91-8 ]
Reference: [1] Industrial and Engineering Chemistry, 1948, vol. 40, p. 507
[2] Journal of the Chemical Society, 1947, p. 1519
[3] Journal of the American Chemical Society, 1951, vol. 73, p. 3814
[4] Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1976, vol. 30, p. 21 - 23
[5] Acta Chemica Scandinavica (1947-1973), 1970, vol. 24, p. 1241 - 1246
  • 3
  • [ 762-98-1 ]
  • [ 7328-91-8 ]
  • [ 41882-44-4 ]
Reference: [1] Journal of the American Chemical Society, 1949, vol. 71, p. 3250
[2] Patent: US2418237, 1944, ,
  • 4
  • [ 41882-44-4 ]
  • [ 7328-91-8 ]
Reference: [1] Journal of Medicinal Chemistry, 1995, vol. 38, # 19, p. 3789 - 3797
  • 5
  • [ 922-84-9 ]
  • [ 7328-91-8 ]
Reference: [1] Patent: US4665210, 1987, A,
  • 6
  • [ 126-30-7 ]
  • [ 26734-09-8 ]
  • [ 7328-91-8 ]
Reference: [1] Angewandte Chemie - International Edition, 1999, vol. 38, # 3, p. 351 - 354
  • 7
  • [ 5659-93-8 ]
  • [ 7328-91-8 ]
Reference: [1] Journal of Medicinal Chemistry, 1995, vol. 38, # 19, p. 3789 - 3797
  • 8
  • [ 31044-89-0 ]
  • [ 7328-91-8 ]
Reference: [1] Journal of Organic Chemistry, 1971, vol. 36, p. 3042 - 3044
  • 9
  • [ 31044-87-8 ]
  • [ 7328-91-8 ]
Reference: [1] Journal of Organic Chemistry, 1971, vol. 36, p. 3042 - 3044
  • 10
  • [ 126-30-7 ]
  • [ 7328-91-8 ]
Reference: [1] Journal of Organic Chemistry, 1971, vol. 36, p. 3042 - 3044
  • 11
  • [ 67744-70-1 ]
  • [ 7328-91-8 ]
Reference: [1] Journal of the Chemical Society, 1947, p. 1502[2] Chem.Abstr., 1948, p. 770
  • 12
  • [ 114583-17-4 ]
  • [ 7328-91-8 ]
Reference: [1] Journal of the Chemical Society, 1947, p. 1502[2] Chem.Abstr., 1948, p. 770
  • 13
  • [ 762-98-1 ]
  • [ 7328-91-8 ]
  • [ 41882-44-4 ]
Reference: [1] Journal of the American Chemical Society, 1949, vol. 71, p. 3250
[2] Patent: US2418237, 1944, ,
  • 14
  • [ 7328-91-8 ]
  • [ 24424-99-5 ]
  • [ 292606-35-0 ]
YieldReaction ConditionsOperation in experiment
31.6% at 0 - 20℃; for 12 h; To a solution of 2,2-dimethylpropane-1 ,3-diamine (80 g, 783 mmol) in dichloromethane (DCM) (500 mL) at 0 °C was added Boc-anhydride (91 ml_, 391 mmol). It was stirred at ambient temperature for 12 h. The reaction mixture was concentrated. The crude product was purified with column chromatography (Neutral Allumina) by using MeOH : DCM (1 :9) as solvent to give the title compound (50 g, 247 mmol, 31 .6 percent yield) as a white solid. 1H NMR (400 MHz, CDC ) δ ppm 0.85 (s, 6 H), 1 .44 (s, 9 H), 2.35 - 2.52 (m, 2 H), 3.00 (br d, J=6.14 Hz, 2 H), 5.16 (br s, 1 H). tert-Butyl (2,2-dimethyl-3-(2-nitrophenylsulfonamido)propyl)carbamate
Reference: [1] Patent: WO2018/109648, 2018, A1, . Location in patent: Page/Page column 64
[2] Journal of Medicinal Chemistry, 1998, vol. 41, # 2, p. 236 - 246
[3] Patent: US2005/20623, 2005, A1, . Location in patent: Page 116
[4] Patent: EP1550657, 2005, A1, . Location in patent: Page/Page column 46
  • 15
  • [ 7328-91-8 ]
  • [ 292606-35-0 ]
Reference: [1] Patent: US2012/178772, 2012, A1,
[2] Chemistry - A European Journal, 2014, vol. 20, # 25, p. 7706 - 7717
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