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Chemical Structure| 73963-42-5 Chemical Structure| 73963-42-5

Structure of 73963-42-5

Chemical Structure| 73963-42-5

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Product Details of [ 73963-42-5 ]

CAS No. :73963-42-5
Formula : C11H19ClN4
M.W : 242.75
SMILES Code : ClCCCCC1=NN=NN1C2CCCCC2
MDL No. :MFCD01076191
InChI Key :INTQSGGUSUSCTJ-UHFFFAOYSA-N
Pubchem ID :11218739

Safety of [ 73963-42-5 ]

GHS Pictogram:
Signal Word:Danger
Hazard Statements:H228-H315-H319
Precautionary Statements:P210-P241-P264-P280-P362
Class:4.1
UN#:1325
Packing Group:

Application In Synthesis of [ 73963-42-5 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 73963-42-5 ]

[ 73963-42-5 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 5470-65-5 ]
  • [ 73963-42-5 ]
  • C17H22BrN5O3 [ No CAS ]
YieldReaction ConditionsOperation in experiment
90% With sodium hydroxide; In butan-1-ol; for 8h;Reflux; 1. In a 250 ml three-necked round bottom flask, add 21.8 g (0.1 mol) of <strong>[5470-65-5]p-nitro-3-bromophenol</strong>, 8 g (0.2 mol) of sodium hydroxide, and 1-cyclohexyl-5-(4-chlorobutyl)-1H-tetrazole 48.5 g (0.2 mol) and n-butanol 150 ml.After refluxing for 8 h, the reaction was completed by TLC. The reaction mixture was cooled to room temperature, water and ethyl acetate were added, and the organic phase was separated and washed with water and brine, Dried and concentrated under reduced pressure,The obtained residue was recrystallized from ethanol, and the precipitate was collected by filtration.Drying to give the compound138.1 g, the purity is 98% or more, and the yield is 90%.
 

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